1-硝基-4-[(1e)-2-硝基-1-丙烯-1-基]苯合成路线 （共 13 条）
反应条件
potassium carbonate in acetonitrile T=20°C; 24 h;
参考文献
Chen, Zhan-Guo; Zhao, Peng-Fei; Wang, Yun
European Journal of Organic Chemistry, 2011 , # 29 p. 5887 - 5893
反应条件
2-HEAF
T=20°C; Knoevenagel condensation; 2.2 h; Ionic liquid;
参考文献
Alizadeh, Abdolhamid; Khodaei, Mohammad M.; Eshghi, Ali
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8295 - 8298
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
0.75 h;
参考文献
Denmark, Scott E.; Kesler, Brenda S.; Moon, Young-Choon
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 4912 - 4924
反应条件
C13H25N3O2
T=5°C; Henry reaction; 48 h;
参考文献
Rodriguez-Llansola, Francisco; Escuder, Beatriu; Miravet, Juan F.
Journal of the American Chemical Society, 2009 , vol. 131, # 32 p. 11478 - 11484
反应条件
ammonium acetate in acetic acid
P=760 Torr; 2 h; Heating;
参考文献
Agafonov, N. E.; Sedishev, I. P.; Dudin, A. V.; Kutin, A. A.; Stashina, G. A.; Zhulin, V. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 2.2 p. 366 - 372
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 2 p. 426 - 433
反应条件
1: 88 percent / DMAP / diethyl ether / 3 h
2: 77 percent / DMAP / CH2Cl2 / 0.75 h
View Scheme
参考文献
Denmark, Scott E.; Kesler, Brenda S.; Moon, Young-Choon
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 4912 - 4924
反应条件
1: 78 percent / t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran
2: 88 percent / DMAP / diethyl ether / 3 h
3: 77 percent / DMAP / CH2Cl2 / 0.75 h
View Scheme
参考文献
Denmark, Scott E.; Kesler, Brenda S.; Moon, Young-Choon
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 4912 - 4924
反应条件
in acetonitrile
T=30°C; var. temp.; Equilibrium constant;
参考文献
Shunmugasundaram, A; Thanulingam, T Lekshmana; Murugesan, R
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1991 , vol. 30, # 7 p. 609 - 613
反应条件
hydrogenchloride; potassium hydroxide
1) ether, reflux, 2) methanol, water, 0.5 h, reflux; Yield given. Multistep reaction;
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Ruhr, Maria
Liebigs Annalen der Chemie, 1985 , # 2 p. 239 - 250
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Redelfs, Elke; Ruhr, Maria
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 1853 - 1859
