反应条件
1: 1,1,2,2,3,3,4,4,4-nonafluoro-1-iodobutane With ethyl bromide; magnesium in diethyl ether
T=-40 - -20°C; Inert atmosphere;
2: chlorobenzene With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in diethyl ether
T=-20 - 35°C; Grignard reaction; Inert atmosphere;
参考文献
Blom, Elisabeth; Karimi, Farhad; Langstroem, Bengt
Journal of Labelled Compounds and Radiopharmaceuticals, 2010 , vol. 53, # 1 p. 24 - 30
