alpha-乙基呋喃-2-甲醇合成路线 （共 20 条）
反应条件
iodine distillation;
参考文献
Lapidus, A. L.; Rodin, A. P.; Pruidze, I. G.; Ugrak, B. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 7.2 p. 1509 - 1511
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 7 p. 1661 - 1662
反应条件
[bis(acetoxy)iodo]benzene; BF4(1-)*C19H32N6O2(1+) in dichloromethane T=20°C; 0.05 h;
参考文献
Fall, Alioune; Sene, Massene; Gaye, Mohamed; Gomez, Generosa; Fall, Yagamare
Tetrahedron Letters, 2010 , vol. 51, # 34 p. 4501 - 4504
反应条件
T=175°C; Hydrogenation;
参考文献
Douris
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1913 , vol. 157, p. 723
反应条件
unter Druck.Hydrogenation;
参考文献
Pierce; Adams
Journal of the American Chemical Society, 1925 , vol. 47, p. 1103
参考文献
Bukharov,V.G.; Pozdnyakova,T.E.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1960 , # 6 p. 1031 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , # 6 p. 1108 - 1113
反应条件
chlorine in methanol; water 1.) -5 deg C; 2.) 90-95 deg C, 3.5 h;
参考文献
Georgiadis, Minas P.; Albizati, Kim F.; Georgiadis, Taxiarchis M.
Organic Preparations and Procedures International, 1992 , vol. 24, # 1 p. 95 - 118
反应条件
tetra-n-butyl phosphonium chloride in toluene
T=0 - 23°C; Inert atmosphere; chemoselective reaction;
参考文献
Werner, Thomas; Riahi, Abdol Majid; Schramm, Heiko
Synthesis, 2011 , # 21 art. no. N59811SS, p. 3482 - 3490
反应条件
isoprene; bis(acetylacetonate)nickel(II) in tetrahydrofuran; hexane
1 h; Ambient temperature; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kimura, Masanari; Fujimatsu, Hidetaka; Ezoe, Akihiro; Shibata, Kazufumi; Shimizu, Masamichi; Matsumoto, Satoru; Tamaru, Yoshinao
Angewandte Chemie - International Edition, 1999 , vol. 38, # 3 p. 397 - 400
反应条件
bis(acetylacetonate)nickel(II); diethylzinc in tetrahydrofuran; hexane
T=0°C; 1 h; Title compound not separated from byproducts;
参考文献
Kimura, Masanari; Ezoe, Akihiro; Mori, Masahiko; Iwata, Keisuke; Tamaru, Yoshinao
Journal of the American Chemical Society, 2006 , vol. 128, # 26 p. 8559 - 8568
反应条件
isopropyl alcohol; [{RuCl(μ-Cl)(η6-C6Me6)}2]
T=82°C; 5 h;
参考文献
Cadierno, Victorio; Francos, Javier; Gimeno, Jose; Nebra, Noel
Chemical Communications, 2007 , # 24 p. 2536 - 2538
