反-3,5-二甲氧基-4-羟基肉桂合成路线 （共 13 条）
反应条件
lithium tri-t-butoxyaluminum hydride; copper(l) iodide T=-78°C; 1 h;
参考文献
Duran, E.; Gorrichon, L.; Cazaux, L.; Tisnes, P.
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2755 - 2758
反应条件
potassium hydroxide in ethanol 12 h;
参考文献
Daubresse; Francesch; Mhamdi; Rolando
Synthesis, 1994 , # 4 p. 369 - 371
反应条件
1: 1.) aqueous potassium carbonate, 2.) 10percent aq. HCl / 1.) tris-<2-(2-methoxyethoxy)ethyl>amine / 1.) dichloromethane, room temperature, 12 h, 2.) dichloromethane, room temperature, 12 h 2: 86 percent / KOH / aq. ethanol / 12 h View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
2: 74 percent / LiAl(OBu)3H / CuI / 1 h / -78 °C View Scheme
参考文献
Duran, E.; Gorrichon, L.; Cazaux, L.; Tisnes, P.
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2755 - 2758
反应条件
1,4-dioxane; quinoline; Pd-BaSO4 Hydrogenation.Reagens 4:Xylol;Behandeln des Reaktionsprodukts in CHCl3 mit Natriummethylat in Methanol;
参考文献
Pearl
Journal of Organic Chemistry, 1959 , vol. 24, p. 736,738
反应条件
1: SOCl2 2: lithium-<tri-tert-butoxy-alanate>; THF View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
1: pyridine; SOCl2 2: palladium/BaSO4; xylene / Hydrogenation 3: aniline; pyridine 4: pyridine; SOCl2 5: palladium/BaSO4; dioxane; quinoline / Hydrogenation.Reagens 4:Xylol;Behandeln des Reaktionsprodukts in CHCl3 mit Natriummethylat in Methanol View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
反应条件
1: palladium/BaSO4; xylene / Hydrogenation 2: aniline; pyridine 3: pyridine; SOCl2 4: palladium/BaSO4; dioxane; quinoline / Hydrogenation.Reagens 4:Xylol;Behandeln des Reaktionsprodukts in CHCl3 mit Natriummethylat in Methanol View Scheme
参考文献
Freudenberg; Huebner
Chemische Berichte, 1952 , vol. 85, p. 1181,1188
参考文献
Gapan'kova; Brinkevich; Edimecheva; Kurchenko; Shadyro
High Energy Chemistry, 2011 , vol. 45, # 3 p. 196 - 201
反应条件
sodium tetrahydroborate in ethyl acetate 1 h; Ambient temperature;
参考文献
Ludley, Frank H.; Ralph, John
Journal of Agricultural and Food Chemistry, 1996 , vol. 44, # 10 p. 2942 - 2943
