2-环己基-1,4-苯二醇合成路线 （共 11 条）
反应条件
palladium on activated charcoal T=370°C; Kinetics; Further Variations:Temperatures;
参考文献
Kuznetsova; Postnova; Koshel'; Lebedeva; Yun'kova
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 9 p. 1288 - 1290
参考文献
Flaig et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 597, p. 196,211
反应条件
1: cyclohexene With dimethylsulfide borane complex in dimethylsulfide; dichloromethane
T=0°C; 3 h; Inert atmosphere;
2: With 2-benzyl-1,2,3,4-tetrahydroisoquinoline-6,7-diol in dimethylsulfide; dichloromethane
T=0 - 20°C; Inert atmosphere;
3: p-benozquinone With N,N'-dimethyl-N,N'-propyleneurea in dimethylsulfide; dichloromethane
T=20°C; 2 h; Inert atmosphere;
参考文献
Luethy, Monique; Darmency, Vincent; Renaud, Philippe
European Journal of Organic Chemistry, 2011 , # 3 p. 547 - 552
反应条件
in tetrahydrofuran; diethyl ether; hexane
T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Zillman, David J.; Hincapie, Gloria C.; Reza Savari; Mizori, Farhad G.; Cole, Thomas E.
Tetrahedron Letters, 2010 , vol. 51, # 23 p. 3033 - 3036
反应条件
N,N'-dimethyl-N,N'-propyleneurea; water in dichloromethane
T=25°C; 2 h;
参考文献
Kumli, Eveline; Montermini, Florian; Renaud, Philippe
Organic Letters, 2006 , vol. 8, # 25 p. 5861 - 5864
反应条件
1: N,N-dimethylacetamide / CH2Cl2 / 5 h / Heating
2: water; DMPU / CH2Cl2 / 2 h / 25 °C
View Scheme
参考文献
Kumli, Eveline; Montermini, Florian; Renaud, Philippe
Organic Letters, 2006 , vol. 8, # 25 p. 5861 - 5864
反应条件
phosphoric acid
T=130°C;
参考文献
Postnova; Koshel'; Lebedeva; Kuznetsova
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 10 p. 1415 - 1417
参考文献
Flaig et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 597, p. 196,211
反应条件
1: P2O5 / Erhitzen des Reaktionsprodukts mit Acetanhydrid unter Zusatz von Zink-Pulver
2: methanol. HCl
View Scheme
参考文献
Flaig et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 597, p. 196,211
反应条件
1: P2O5 / Erhitzen des Reaktionsprodukts mit Acetanhydrid unter Zusatz von Zink-Pulver
2: methanol. HCl
View Scheme
参考文献
Flaig et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 597, p. 196,211
