1-甲磺酰基-2-咪唑烷酮合成路线 (共 7 条)
反应条件
sodium hydride in benzene 6 h; Heating;
参考文献
Atanassova; Nakov; Pavlova
Pharmazie, 1991 , vol. 46, # 9 p. 670 - 671
反应条件
in dichloromethane 0.75 h; Ambient temperature;
参考文献
Atanassova; Nakov; Pavlova
Pharmazie, 1991 , vol. 46, # 9 p. 670 - 671
参考文献
Bayer Aktiengesellschaft
Patent: US3972870 A1, 1976 ;
反应条件
pyridine in chloroform T=50 - 55°C; Addition; 3 h;
参考文献
Su, Weike; Huang, Kewei; Zhang, Yongmin
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 498 - 501
反应条件
in chloroform T=55 - 60°C; chloroformylation; 3 h;
参考文献
Su; Zhang
Journal of Chemical Research - Part S, 2000 , # 9 p. 440 - 441
反应条件
sodium hydride in N,N-dimethyl-formamide
T=25°C; 5 h;
参考文献
Nagarajan, K.; Arya, V. P.; George, T.; Sudarsanam, V.; Shah, R. K.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 10 p. 928 - 940
反应条件
sodium hydride in N,N-dimethyl-formamide
1.) 30 min, room temperature, 2.) a) 1 h, room temperture, b) 3 h, 55 deg C, c) room temperature;
参考文献
Sudarsanam, V.; Nagarajan, K.; George, T.; Shenoy, S. J.; Iyer, V. V.; Kaulgud, A. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 11 p. 1022 - 1026