(1,1-二乙基丙基)苯合成路线 (共 12 条)
反应条件
anthracene; sodium
T=200 - 225°C; P=22065.2 Torr;
参考文献
Rylander; Meyerson
Journal of the American Chemical Society, 1956 , vol. 78, p. 5799,5802
反应条件
Et2Al[HCB11H5Br6] in hexanes
T=20°C; 24 h; Inert atmosphere;
参考文献
Gu, Weixing; Haneline, Mason R.; Douvris, Christos; Ozerov, Oleg V.
Journal of the American Chemical Society, 2009 , vol. 131, # 31 p. 11203 - 11212
反应条件
1: phenyl-(9-BBN) With lithium tert-butylate in 2-methyl-propan-1-ol; benzene
T=20°C; 0.333333 h; Schlenk techniqueInert atmosphere;
2: triethylcarbinyl bromide With [(diglyme)NiBr2]; 4,4'-di-tert-butyl-2,2'-dipyridyl in 2-methyl-propan-1-ol; benzene
T=20 - 40°C; Suzuki Coupling; 28.5 h; Schlenk techniqueInert atmosphere;
参考文献
Zultanski, Susan L.; Fu, Gregory C.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 624 - 627
反应条件
aluminium trichloride
T=20 - 30°C;
参考文献
Huston; Fox; Binder
Journal of Organic Chemistry, 1938 , vol. 3, p. 252
反应条件
aluminium trichloride; nitrobenzene
T=20°C;
参考文献
Grundy et al.
Journal of the Chemical Society, 1958 , p. 581,584
反应条件
1: HCl
2: AlCl3
View Scheme
参考文献
Schreiner
Journal fuer Praktische Chemie (Leipzig), 1910 , vol. <2>82, p. 292
反应条件
aluminium trichloride
参考文献
Schreiner
Journal fuer Praktische Chemie (Leipzig), 1910 , vol. <2>82, p. 292
参考文献
Baas,J.M.A.; Wepster,B.M.
Recueil des Travaux Chimiques des Pays-Bas, 1972 , vol. 91, p. 517 - 527
参考文献
Huston; Fox; Binder
Journal of Organic Chemistry, 1938 , vol. 3, p. 252
参考文献
Grundy et al.
Journal of the Chemical Society, 1958 , p. 581,584