1,1-二甲氧基-2-甲基丙烷合成路线 （共 28 条）
反应条件
zinc(II) chloride in toluene T=80°C; 5 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
ozone in ethyl acetate T=-40°C; ΔH, ΔS; Rate constantThermodynamic data;
参考文献
Taillefer, Roland J.; Thomas, Shirley E.; Nadeau, Yves; Fliszar, S.; Henry, Herve
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1138 - 1143
反应条件
1.) bromination, 2.) dehydrohalogenation; Multistep reaction;
参考文献
Molenaar-Langeveld, Tineke A.; Fokkens, Roel H.; Nibbering, Nico M. M.
Organic Mass Spectrometry, 1988 , vol. 23, p. 364 - 369
反应条件
manganese(IV) oxide; chloro-trimethyl-silane; manganese (II) chloride in methanol; acetonitrile T=40°C; 6 h;
参考文献
Tetrahedron, , vol. 48, # 22 p. 4579 - 4586
反应条件
water; toluene-4-sulfonic acid; triethylamine T=90°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
Kyowa Hakko Chemical Co., Ltd.
Patent: EP1876163 A1, 2008 ;
Location in patent: Page/Page column 4 ;
反应条件
water T=25°C; ΔH(liq)=8698 cal/mol; Thermodynamic data;
参考文献
Wiberg, Kenneth B.; Squires, Robert R.
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4473 - 4478
反应条件
sodium methylate; toluene-4-sulfonic acid; toluene-4-sulfonic acid
1.) 0 deg C, 30 min., 2.) room temp, overnight;
参考文献
Hamon, David P. G.; Trenerry, Craige V.
Australian Journal of Chemistry, 1980 , vol. 33, # 4 p. 809 - 821
反应条件
ammonia; titanium tetrachloride in dichloromethane
T=0°C; other reagent (Et3N); Product distribution;
参考文献
Clerici, Angelo; Pastori, Nadia; Porta, Ombretta
Tetrahedron, 1998 , vol. 54, # 51 p. 15679 - 15690
反应条件
hydrogen azide; titanium tetrachloride in dichloromethane
3 h; Ambient temperature;
参考文献
Hassner, Alfred; Fibiger, Richard; Amarasekara, Ananda S.
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 22 - 27
反应条件
KU-2 resin
T=40°C; 5 h;
参考文献
Gazizova, L. B.; Imashev, U. B.; Musavirov, R. S.; Kantor, E. A.; Zlotskii, S. S.; et al.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 226 - 231
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 275 - 281
