1-(4-氯苯基)-3,3-双甲基磺酰基丙酮合成路线 （共 9 条）
参考文献
Sharon, Ashoke; Pratap, Ramendra; Maulik, Prakas R.; Ram, Vishnu Ji
Tetrahedron, 2005 , vol. 61, # 15 p. 3781 - 3787
反应条件
sodium 1.) THF, 2.) reflux, 1 d; Yield given. Multistep reaction;
参考文献
Huang, Zhi-Tang; Zhang, Ping-Cheng
Synthetic Communications, 1989 , vol. 19, # 17 p. 2999 - 3006
反应条件
1: para-chloroacetophenone With potassium tert-butylate in tetrahydrofuran
T=20°C; 0.25 h;
2: carbon disulfide; methyl iodide in tetrahydrofuran
T=20°C; 10 h;
参考文献
Lubbe, Mathias; Klassen, Renske; Trabhardt, Tiana; Villinger, Alexander; Langer, Peter
Synlett, 2008 , # 15 p. 2331 - 2333
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in tetrahydrofuran
T=20°C; 1.5 h; or with irradiation (UV);
参考文献
Lakeev, S. I.; Galin, F. Z.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 1.2 p. 202
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 38, # 1 p. 213 - 214
反应条件
carbon disulfide; sodium hydride
Multistep reaction;
参考文献
Huang, Zhi-Tang; Zhang, Ping-Cheng
Synthetic Communications, 1990 , vol. 20, # 9 p. 1399 - 1407
参考文献
Thuillier; Vialle
Bulletin de la Societe Chimique de France, 1959 , p. 1398,1400
参考文献
Clesse,F.; Quiniou,H.
Bulletin de la Societe Chimique de France, 1973 , p. 581 - 585
反应条件
CuCl2·2H2O
T=90°C; Knoevenagel cyclocondensation; 0.166667 h; Neat (no solvent);
参考文献
Singh, Okram Mukherjee; Devi, Nepram Sushuma; Devi, Laishram Ronibala; Lim, Ki Bum; Yoon, Yong Jin; Lee, Sang-Geyong
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 175 - 178
反应条件
1: 98 percent / NBS / CCl4 / 1.5 h / Ambient temperature
2: 78 percent / various solvent(s); pyridine / 1 h / 180 - 190 °C
View Scheme
参考文献
Singh, Gurdeep; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Synthesis, 1985 , # 2 p. 165 - 169
