4-氯甲基-6-甲基-苯并吡喃-2-酮合成路线 (共 5 条)
反应条件
sulfuric acid in water T=20°C; 18 h;
参考文献
WO2008/74752 A2, ;
Page/Page column 38 ;
WO 2008/074752 A2
反应条件
phosphorus pentachloride in benzene 4 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 21, # 5 p. 399 - 402
反应条件
1: 80 percent / SeO2 / xylene / 12 h / Heating 2: 0.4 g / NaBH4 / methanol / 0.5 h / T < 40 deg C 3: PCl5 / benzene / 4 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 21, # 5 p. 399 - 402
反应条件
1: 0.4 g / NaBH4 / methanol / 0.5 h / T < 40 deg C 2: PCl5 / benzene / 4 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 21, # 5 p. 399 - 402
反应条件
chlorine; acetic acid
参考文献
Journal of the Indian Chemical Society, , vol. 11, p. 635,648