in hexane; cyclohexane
to p-bromotoluene (1.02 mmol) and Me3SnH (2.04 mmol) in hexane at 0°C added LDA (1 mmol, in cyclohexane) under Ar, react. time 20 min, quenched with water; analyzed by GLPC;
参考文献
Reimann, Werner; Kuivila, Henry G.; Farah, Dan; Apoussidis, Theodorus
Organometallics, 1987 , vol. 6, p. 557 - 565
in diethyl ether; cyclohexane
byproducts: i-Pr2NH; Et3SnH in Et2O cooled to 0°C under Ar, LDA in cyclohexane (1.6 M) added via syringe, stirred for 60 min at room temp., hydrolysis;
参考文献
Reimann, Werner; Kuivila, Henry G.; Farah, Dan; Apoussidis, Theodorus
Organometallics, 1987 , vol. 6, p. 557 - 565
