2',3',5'-三乙酰尿苷合成路线 （共 45 条）
反应条件
4-(N,N-dimethlyamino)pyridine
参考文献
Park, Sun Min; Shen, Yongcun; Kim, Byeang Hyean
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 4 p. 610 - 612
反应条件
3,3-dimethyldioxirane in dichloromethane; acetone T=25°C;
参考文献
Crestini; Saladino; Bernini; Mincione
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7785 - 7788
反应条件
sodium iodide in acetone T=20°C; Reduction; 24 h;
参考文献
Serra, Carme; Farras, Jaume; Vilarrasa, Jaume
Tetrahedron Letters, 1999 , vol. 40, # 51 p. 9111 - 9113
反应条件
1: [131I]-Uracil With N,O-bis-(trimethylsilyl)-acetamide in acetonitrile T=20°C; 0.5 h; 2: 2,3,5-tri-O-acetyl-D-ribofuranosyl 1-(N-phenyl)-2,2,2-trifluoroacetimidate With trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane T=20°C; Further stages.;
参考文献
Liao, Jinxi; Sun, Jiansong; Yu, Biao
Tetrahedron Letters, 2008 , vol. 49, # 34 p. 5036 - 5038
反应条件
1: With N,O-bis(trimethylsilyl) trifluoroacetamide in acetonitrile T=20°C; 0.5 h; Inert atmosphere; 2: With Au(Ph3P)+NTf2- in acetonitrile T=20°C; Inert atmosphere;
参考文献
Zhang, Qingju; Sun, Jiansong; Zhu, Yugen; Zhang, Fuyi; Yu, Biao
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4933 - 4936
反应条件
trimethylsilyl trifluoromethanesulfonate; 1,1,1,3,3,3-hexamethyl-disilazane; 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide in acetonitrile Vorbrueggen Nucleoside Synthesis; Microwave irradiation;
参考文献
Parmenopoulou, Vanessa; Chatzileontiadou, Demetra S.M.; Manta, Stella; Bougiatioti, Stamatina; Maragozidis, Panagiotis; Gkaragkouni, Dimitra-Niki; Kaffesaki, Eleni; Kantsadi, Anastassia L.; Skamnaki, Vassiliki T.; Zographos, Spyridon E.; Zounpoulakis, Panagiotis; Balatsos, Nikolaos A.A.; Komiotis, Dimitris; Leonidas, Demetres D.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 24 p. 7184 - 7193
反应条件
trifluoroacetic acid T=25°C; 24 h;
参考文献
DeFrees, Shawn A.; Reddy, Kalakota S.; Cassady, John M.
Synthetic Communications, 1988 , vol. 18, # 2 p. 213 - 220
反应条件
3,3-dimethyldioxirane in ethanol; dichloromethane; acetone T=25°C;
参考文献
Saladino, Raffaele; Crestini, Claudia; Occhionero, Francesca; Nicoletti, Rosario
Tetrahedron, 1995 , vol. 51, # 12 p. 3607 - 3616
反应条件
3,3-dimethyldioxirane in ethanol; dichloromethane; acetone T=25°C;
参考文献
Saladino, Raffaele; Crestini, Claudia; Occhionero, Francesca; Nicoletti, Rosario
Tetrahedron, 1995 , vol. 51, # 12 p. 3607 - 3616
反应条件
water in ethylene glycol dimethyl ether T=125°C; 9 h;
参考文献
Nowak, Ireneusz; Robins, Morris J.
Organic Letters, 2005 , vol. 7, # 22 p. 4903 - 4905
