tert.-butyl lithium in pentane byproducts: hexamethyldistannane; under argon; reaction time: 1-48 h; at -78 or -100 ° C; to mixture of TMEDA and LiBu addn. (-78 °C) of C8H10 (all at once), cooling is finished; after 24 h solution is cooled to -78 °C and Me3SnCl was added;; addition of H2O at 0 °C; extraction (pentane); evaporation of pentane; distillation (vacuum); elem. anal.; further products;
参考文献
Hertkorn, N.; Koehler, F. H.
Journal of Organometallic Chemistry, 1988 , vol. 355, p. 19 - 32