2-氯-5,5-二甲基-1,3,2-二氧磷杂环己烷 2-氧化物合成路线 （共 31 条）
反应条件
ammonia; sodium in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
Nycz, Jacek; Rachon, Janusz
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 161, p. 39 - 59
反应条件
in tetrahydrofuran T=20°C; 1 h;
参考文献
Patois, Carl; Ricard, Louis; Savignac, Philippe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1577 - 1581
反应条件
water T=50°C; Kinetics;
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
参考文献
Edmundson,R.S.
Tetrahedron, 1964 , vol. 20, p. 2781 - 2795
反应条件
triethylamine in toluene Yield given;
参考文献
Raghu; Devendranath Reddy
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 11 p. 1228 - 1232
反应条件
triethylamine; trichlorophosphate in dichloromethane
T=0°C; 0.5 h;
参考文献
Yamada, Takeshi; Takemura, Kazunobu; Yoshida, Jun-Ichi; Yamago, Shigeru
Angewandte Chemie - International Edition, 2006 , vol. 45, # 45 p. 7575 - 7578
反应条件
trichlorophosphate in toluene
T=50 - 75°C; 2 h;
参考文献
DAIHACHI CHEMICAL INDUSTRY CO., LTD.
Patent: EP1808437 A1, 2007 ;
Location in patent: Page/Page column 13-14; 17 ;
反应条件
1: benzene
2: 76 percent / benzene / 3 h / Ambient temperature
3: Cl-CN / CH2Cl2 / 72 h / Ambient temperature
View Scheme
参考文献
Uznanski, B.; Stec, W. J.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 6 p. 1225 - 1235,1093 - 1102
反应条件
1: 76 percent / benzene / 3 h / Ambient temperature
2: Cl-CN / CH2Cl2 / 72 h / Ambient temperature
View Scheme
参考文献
Uznanski, B.; Stec, W. J.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 6 p. 1225 - 1235,1093 - 1102
