2,2'-氧基二[5,5-二甲基-1,3,2-二氧杂磷杂环己烷] 2,2'-二硫化物合成路线 （共 2 条）
反应条件
thiophosphoryl trichloride; water
T=50 - 60°C; Product distribution / selectivity;
参考文献
LONZA LTD.; PARADIES, Gesa; RIEDEL, Thomas; SCHNIDER, Christian
Patent: WO2010/49083 A1, 2010 ;
Location in patent: Page/Page column 5 ;
反应条件
triphenylphosphine in dichloromethane
1.) -70 deg C -> room temperature, 2.) room temperature, 30 min; Title compound not separated from byproducts;
参考文献
Krawczyk, Ewa; Skowronska, Aleksandra; Michalski, Jan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 89 - 100
