1: sodium methoxide / methanol / 0.33 h / Ambient temperature; deprotection
2: 79 percent / sodium hydride / tetrahydrofuran / 12 h / Ambient temperature
View Scheme
参考文献
Dhanak, Dashyant; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 2181 - 2186
1: 95 percent / potassium hydroxide / H2O; tetrahydrofuran / 1 h / Heating
2: 79 percent / sodium hydride / tetrahydrofuran / 12 h / Ambient temperature
View Scheme
参考文献
Dhanak, Dashyant; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 2181 - 2186