View Scheme

aqueous alkali

暂无反应条件数据

暂无反应条件数据

chloroform; ammonia

1.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere 2.1: potassium carbonate / acetone / 18 h / Reflux 3.1: N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium / diethyl ether / 1 h / -78 °C / Inert atmosphere 3.2: 0.83 h / -78 - 20 °C / Inert atmosphere 3.3: 0 °C / pH 5 - 6 / Inert atmosphere 4.1: sodium tetrahydroborate / methanol / 0.75 h / 0 - 20 °C / Inert atmosphere 5.1: hydrogenchloride / methanol; water / 16 h / 0 °C / pH 4 - 5 / Inert atmosphere; Reflux 6.1: 1-trans-IODO-4-CYCLOHEXYL / N,N-dimethyl-formamide / 78 h / Reflux; Inert atmosphere View Scheme

thionyl chloride in chloroform Heating;

1.1: potassium carbonate / 4 h / |Reflux 2.1: sodium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 1.5 h / 10 - 20 °C 2.2: 0.08 h 3.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C View Scheme

1.1: sodium dihydrogenphosphate; dihydrogen peroxide; sodium chlorite / water; acetonitrile / 1.5 h / 10 - 20 °C 1.2: 0.08 h 2.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C View Scheme

benzene