4,16-雄二烯-3-酮 合成路线 (共 18 条)
参考文献
Pherin Pharmaceuticals, Inc.
Patent: US6117860 A1, 2000 ;
反应条件
1: With tetra-n-butylammonium acetate in 1-methyl-pyrrolidin-2-one T=160°C; 4 h; 2: With potassium hydroxide in ethanol T=20°C; 48 h;
参考文献
Hantos, Susanne M.; Tripathy, Sasmita; Alibhai, Najma; Durst, Tony
Canadian Journal of Chemistry, 2001 , vol. 79, # 11 p. 1747 - 1753
反应条件
copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; potassium carbonate in dimethyl sulfoxide T=100°C; 24 h; Inert atmosphere; Reagent/catalystSolventTemperature;
参考文献
European Journal of Organic Chemistry, , # 34 p. 7823 - 7832
反应条件
18-crown-6 ether; caesium acetate in benzene 72 h; Heating;
参考文献
Tetrahedron Letters, , vol. 37, # 34 p. 6145 - 6148
反应条件
in water; cyclohexanone; toluene
反应条件
indole; copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide T=100°C; 24 h; Inert atmosphere; Reagent/catalyst;
参考文献
Kotovshchikov, Yury N.; Latyshev, Gennadij V.; Lukashev, Nikolay V.; Beletskaya, Irina P.
European Journal of Organic Chemistry, 2013 , # 34 p. 7823 - 7832
1224-94-8 (3S,8S,9S,10R,13R,14S)-10,13-二甲基-2,3,4,7,8,9,11,12,14,15-十氢-1H-环戊并[a]菲-3-醇
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反应条件
反应条件
cyclohexanone; aluminum isopropoxide; toluene
参考文献
Journal of the American Chemical Society, , vol. 77, p. 4145,4148
反应条件
sodium azide in N,N-dimethyl-formamide T=90°C; Substitution; 0.0833333 h;
参考文献
Synthesis, , # 8 p. 1373 - 1385
反应条件
lithium azide in N,N-dimethyl-formamide T=25°C; Substitution; 0.5 h;
参考文献
Synthesis, , # 8 p. 1373 - 1385