N,N-二甲基-2-苯并噻唑胺合成路线 (共 32 条)
反应条件
1: 97 percent / Cs2CO3 / n-BuPAd2; Pd2dba3 / dioxane / 1 h / 80 °C
View Scheme
参考文献
Benedi, Carolina; Bravo, Fernando; Uriz, Pedro; Fernandez, Elena; Claver, Carmen; Castillon, Sergio
Tetrahedron Letters, 2003 , vol. 44, # 32 p. 6073 - 6077
反应条件
in tetrahydrofuran
T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286
参考文献
Gupton, John T.; Idoux, John P; Baker, Graeme; Colon, Cesar; Crews, A.Donald; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2933 - 2936
反应条件
in tetrahydrofuran
T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286
反应条件
in tetrahydrofuran
T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Toda, Mitsuo; Hashimoto, Shiro
Chemistry Letters, 1991 , # 8 p. 1283 - 1286
反应条件
triethylamine in N,N-dimethyl-formamide
24 h; Heating;
参考文献
El-Faham, Ayman; Chebbo, Mohamed; Abdul-Ghani, Mohamed; Younes, Ghassan
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 3 p. 599 - 606
反应条件
1: triethylamine / dichloromethane / 0.2 h / 20 °C / |Inert atmosphere
2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.23 h / 110 °C / |Inert atmosphere
View Scheme
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
反应条件
Substitution; dealkylation; Heating;
参考文献
Khalaf, Abedawn I; Alvarez, Ricardo G; Suckling, Colin J; Waigh, Roger D
Tetrahedron, 2000 , vol. 56, # 43 p. 8567 - 8571
参考文献
I.G. Farbenind.
Patent: DE617188 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 22, p. 297
参考文献
Nagarajan,K. et al.
Indian Journal of Chemistry, 1971 , vol. 9, p. 748 - 754