3,10-二甲基-苯并(g)蝶啶-2,4(3H,10H)-二酮合成路线 （共 17 条）
反应条件
N-benzyl-trimethylammonium hydroxide in N,N-dimethyl-formamide 6.5 h; Ambient temperaturedarkness;
参考文献
Harayama, Takashi; Tezuka, Yasuhiro; Taga, Tooru; Yoneda, Fumio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 75 - 84
反应条件
in N,N-dimethyl-formamide T=25°C; pH=8.19; Rate constant;
参考文献
Yano, Yumihiko; Ohshima, Masashi; Yatsu, Isao; Sutoh, Susumu; Vasquez, Rafael E.; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 753 - 758
反应条件
oxygen in N,N-dimethyl-formamide
T=120°C; 1 h;
参考文献
Sako; Kojima; Hirota; Maki
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 24, p. 1691 - 1692
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in benzene
T=20°C; 1 h;
参考文献
Geetanjali; Singh, Ram; Chauhan
Synthetic Communications, 2003 , vol. 33, # 4 p. 613 - 620
反应条件
palladium on activated charcoal in decalin
1 h; Heating;
参考文献
Lacroix, Alain; Schabat, Dominique; Clerin, Daniel; Fleury, Jean-Pierre
Bulletin de la Societe Chimique de France, 1987 , # 6 p. 1065 - 1072
反应条件
aluminum oxide
T=110 - 120°C; 0.0666667 h; microwave irradiation;
参考文献
Chauhan; Singh, Ram; Geetanjali
Synthetic Communications, 2003 , vol. 33, # 7 p. 1179 - 1184
反应条件
1: 1.) hydrogen, 2.) sodium nitrite / 1.) palladium/10percent on charcoal / 1.) water, 2.) 1 h
2: 1.) triphenylphosphine, 2.) sodium nitrite, sulfuric acid / 1.) dioxane, 90 min, 2.) 2 h
View Scheme
参考文献
Wessiak; Bruice
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4809 - 4825
反应条件
oxygen in N,N-dimethyl-formamide
2 h; Ambient temperature;
参考文献
Sako; Kojima; Hirota; Maki
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 24, p. 1691 - 1692
反应条件
1: 71 percent / 1.)triethyl amine, 2.) 2N HCl / 1.) acetone, methylene dichloride, 80 deg C, 24h; 2.) chloroform, 48h
2: 97 percent / 10percent Pd/C / decahydronaphthalene / 1 h / Heating
View Scheme
参考文献
Lacroix, Alain; Schabat, Dominique; Clerin, Daniel; Fleury, Jean-Pierre
Bulletin de la Societe Chimique de France, 1987 , # 6 p. 1065 - 1072
反应条件
reduced 3,10-dimethylisoalloxazine in water
T=25°C; pH=6.65;
参考文献
Yano, Yumihiko; Ohshima, Masashi; Yatsu, Isao; Sutoh, Susumu; Vasquez, Rafael E.; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 753 - 758
