2,4,6-三叔丁基硝基苯合成路线 （共 13 条）
反应条件
nitric acid in acetic anhydride; acetic acid 50 h; Ambient temperature;
参考文献
Okada, Tadashi; Karaki, Ichiro; Mataga, Noboru
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7191 - 7195
反应条件
tert.-butylhydroperoxide; cobalt(II)salen in water; 1,2-dichloro-ethane T=23 - 24°C; 2.66667 h;
参考文献
Nishinaga; Forster; Eichhorn; Speiser; Rieker
Tetrahedron Letters, 1992 , vol. 33, # 31 p. 4425 - 4428
反应条件
(t-BuOO)Co(CH2NCHC6H4O)2 in water; 1,2-dichloro-ethane T=23°C; 0.333333 h; other reagents: 1.) PbO2, 2.) tert-butyl hydroperoxide;
参考文献
Foerster, Stefan; Rieker, Anton; Maruyama, Kazushige; Murata, Kunihiko; Nishinaga, Akira
Journal of Organic Chemistry, 1996 , vol. 61, # 10 p. 3320 - 3326
反应条件
1: 1.) AlCl3, 2.) AlCl3 / 1.) room temperature, 19 h 2: 67 percent / HNO3 / acetic anhydride; acetic acid / 50 h / Ambient temperature View Scheme
参考文献
Okada, Tadashi; Karaki, Ichiro; Mataga, Noboru
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7191 - 7195
反应条件
cobalt(II)salen in water; 1,2-dichloro-ethane T=23 - 24°C; 2.66667 h; other substrates; MechanismProduct distribution;
参考文献
Nishinaga; Forster; Eichhorn; Speiser; Rieker
Tetrahedron Letters, 1992 , vol. 33, # 31 p. 4425 - 4428
反应条件
1: aluminium chloride / -3 °C 2: acetic acid; acetic acid anhydride; concentrated nitric acid View Scheme
参考文献
Bartlett et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 2349,2351
反应条件
tert.-butylhydroperoxide; cobalt(II)salen in dichloromethane; water Yield given;
参考文献
Foerster, Stefan; Rieker, Anton; Maruyama, Kazushige; Murata, Kunihiko; Nishinaga, Akira
Journal of Organic Chemistry, 1996 , vol. 61, # 10 p. 3320 - 3326
反应条件
1: 15 percent / <Co(OOC(CH3)3)(o-OC6H4CH=N(CH2)2N=CH-o-C6H4O)> / 1,2-dichloro-ethane; H2O / 0.33 h / 23 °C 2: tert-butyl hydroperoxide, cobalt(II) 1,6-bis(2-hydroxyphenyl)-2,5-diazahexa-1,5-diene complex / CH2Cl2; H2O View Scheme
参考文献
Foerster, Stefan; Rieker, Anton; Maruyama, Kazushige; Murata, Kunihiko; Nishinaga, Akira
Journal of Organic Chemistry, 1996 , vol. 61, # 10 p. 3320 - 3326
反应条件
silver(l) oxide in benzene
参考文献
Inagaki,Y. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 1142 - 1146
反应条件
methanol; sodium amalgam 12 h; Heating;
参考文献
Underiner, Gail E.; Tan, Robin P.; Powell, Douglas R.; West, Robert
Journal of the American Chemical Society, 1991 , vol. 113, # 22 p. 8437 - 8443
