5-碘-1,3-的甲基尿嘧啶合成路线 (共 19 条)
反应条件
(3-methylbut-2-en-1-yl)trimethylsilane in water; acetonitrile Irradiation;
参考文献
Tetrahedron Letters, , vol. 26, # 16 p. 1993 - 1994
反应条件
in water; acetonitrile Irradiation;
参考文献
Tetrahedron Letters, , vol. 26, # 16 p. 1993 - 1994
反应条件
in acetonitrile Irradiation;
参考文献
Tetrahedron Letters, , vol. 21, p. 2813 - 2816
反应条件
in water; acetonitrile 10 h; Ambient temperatureIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5148 - 5153
反应条件
in acetonitrile Irradiation;
参考文献
Tetrahedron Letters, , vol. 21, p. 2813 - 2816
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=100°C; 3.5 h;
参考文献
Havelkova, Martina; Dvorak, Dalimil; Hocek, Michal
Tetrahedron, 2002 , vol. 58, # 37 p. 7431 - 7435
反应条件
1,10-phenanthroline; triethyl amine hydrochloride in N,N-dimethyl-formamide
T=50°C; 12 h; Inert atmosphere;
参考文献
Serizawa, Hiroki; Aikawa, Kohsuke; Mikami, Koichi
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17692 - 17697
反应条件
chloro-trimethyl-silane; ethylene dibromide; zinc
1.) room temperature, 3 h, 2.) THF, 70 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Prasad, A. S. Bhanu; Stevenson, Thomas M.; Citineni, Janakiram Rao; Nyzam, Valerie; Knochel, Paul
Tetrahedron, 1997 , vol. 53, # 21 p. 7237 - 7254
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide
T=90°C; 4 h; Inert atmosphere;
参考文献
Lee, Jae-Young; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7413 - 7416