反应条件
1: 1.) Mg, 1,2-dibromoethane / 1.) Et2O, reflux, 3 h, 2.) Et2O, a) 0 deg C, 5 h, b) RT, overnight 2: 15percent H2O2 / acetone / 4 h / Heating 3: conc. HCl / acetone / 144 h / Ambient temperature View Scheme
参考文献
Hamor, Thomas A.; Jennings, W. Brian; Lovely, Carl J.; Reeves, Keith A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 2 p. 843 - 849