1,1,1,4,4,4-六氟丁烷合成路线 (共 37 条)
反应条件
hydrogen; Lindlar (5percent Pd on CaCO3 poisoned with lead) catalyst T=-78 - 20°C; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: US2008/269532 A1, 2008 ;
Location in patent: Page/Page column 3 ;
反应条件
ethanol; nickel P=73550.8 Torr; Hydrogenation;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: US2008/269532 A1, 2008 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen; palladium/alumina
参考文献
Puy, Michael Van Der; Poss, Andrew J.; Persichini, Phillip J.; Ellis, Lois A. S.
Journal of Fluorine Chemistry, 1994 , vol. 67, # 3 p. 215 - 224
反应条件
sodium hydroxide; hydrogen; palladium in tetrahydrofuran
参考文献
Bayer Aktiengesellschaft
Patent: US4902839 A1, 1990 ;
反应条件
nickel monoaluminide in potassium hydroxide; ethanol
参考文献
Bayer Aktiengesellschaft
Patent: US4902839 A1, 1990 ;
参考文献
Hasek,W.R. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 543 - 551
反应条件
sulfur(IV) fluoride T=20°C; 12 h; steel autoclave;
参考文献
Bloshchitsa, F.A.; Burmakov, A.I.; Kunshenko, B.V.; Alekseeva, L.A.; Yagupol'skii, L.M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 1286 - 1291
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 7 p. 1414 - 1420
反应条件
tritium; quinoline; Lindlar's catalyst P=150 - 500 Torr; 4 h; Ambient temperature;
参考文献
Angelini, G.; Lilla, G.; Sparapani, C.; Ursini, O.; Rossi, E.; et al.
Canadian Journal of Chemistry, 1992 , vol. 70, # 4 p. 1221 - 1228
反应条件
hydrogen; copper on carbon T=310 - 340°C; 0.0188889 - 0.0347222 h; Product distribution / selectivity;
参考文献
E.I.du pont de Nemours and Company
Patent: US2009/12335 A1, 2009 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen; copper on calcium fluoride T=250 - 450°C; 0.0125 h; Product distribution / selectivity;
参考文献
E.I.du pont de Nemours and Company
Patent: US2009/12335 A1, 2009 ;
Location in patent: Page/Page column 6 ;