2-亚甲基环己烷-1-醇合成路线 (共 70 条)
反应条件
RhH2(PPh3)4 T=175°C; 0.5 h; various metall complex catalysts; Product distribution;
参考文献
Felfoeldi, K.; Bartok, M.
Journal of Organometallic Chemistry, 1985 , vol. 297, p. C37 - C40
反应条件
hydrogen; cationic chelate biphosphine rhodium in dichloromethane T=20°C; P=760 Torr;
参考文献
Tetrahedron Letters, , vol. 25, # 13 p. 1393 - 1396
反应条件
hydrogen; cationic chelate biphosphine rhodium in dichloromethane T=20°C; P=760 Torr;
参考文献
Tetrahedron Letters, , vol. 25, # 13 p. 1393 - 1396
反应条件
thionyl chloride in diethyl ether
参考文献
Sato,T.; Homma,I.
Bulletin of the Chemical Society of Japan, 1971 , vol. 44, p. 1885 - 1891
参考文献
Nishida,S. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 939 - 942
反应条件
(i) Zn-Cu, Et2O, (ii) /BRN= 2038531/; Multistep reaction;
参考文献
Tsuji,T. et al.
Bulletin of the Chemical Society of Japan, 1967 , vol. 40, # 10 p. 2338 - 2343
反应条件
methylmagnesium N-cyclohexylisopropylamide in toluene
T=0°C; 20 h;
参考文献
Mosset, Paul; Manna, Sukumar; Viala, Jacques; Falck, J.R.
Tetrahedron Letters, 1986 , vol. 27, # 3 p. 299 - 302
反应条件
1: trimethyl-sulfonium iodide With n-butyllithium in tetrahydrofuran; hexane
T=-10°C; 0.5 h;
2: cyclohexane-1,2-epoxide in tetrahydrofuran; hexane
T=-10 - 20°C; Further stages.;
参考文献
Alcaraz, Lilian; Cridland, Andrew; Kinchin, Elizabeth
Organic Letters, 2001 , vol. 3, # 25 p. 4051 - 4053
反应条件
dichloro-acetic acid; oxygen in acetonitrile
T=25°C; 0.05 h; Irradiationother sensitizers, other solvent, ΔG(excit.); Product distributionThermodynamic dataQuantum yield;
参考文献
Araki; Dobrowolski; Goyne; Hanson; Zhi Qui Jiang; Lee; Foote
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4570 - 4575
反应条件
triethylaluminum in tetrahydrofuran
T=40°C;
参考文献
Wang, Fei; Wang, Shao Hua; Tu, Yong Qiang; Ren, Shi Kuo
Tetrahedron Asymmetry, 2003 , vol. 14, # 15 p. 2189 - 2193