4-氯-1,8-萘二甲酸酐合成路线 （共 20 条）
反应条件
T=220 - 240°C; beim Verschmelzen;
参考文献
Dziewonski; Zakrezewska-Baranowska
Chem. Zentralbl., 1927 , vol. 98, # II p. 427
反应条件
in 2-methoxy-ethanol 6 h; Heating;
参考文献
Beheshtiha; Hekmatshoar; Soltani
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 9 p. 1723 - 1729
反应条件
1: 82 percent / sodium hydroxide, copper / dimethylformamide / 1 h / Heating 2: 94 percent / iron, glacial acetic acid / 1 h / Heating 3: 1.) glacial acetic acid, hydrochloric acid, sodium nitrite, 2.) copper sulphate / 1.) 60 min, 2.) water, reflux, 0.5 h View Scheme
参考文献
Xuhong, Qian; Shengwu, Ren
Journal of Chemical and Engineering Data, 1988 , vol. 33, # 4 p. 528 - 529
反应条件
1: With sodium hydroxide in water T=100°C; 0.0166667 h; microwave irradiation; 2: With mercury(II) diacetate in water T=200°C; Pesci reaction; 0.5 h; microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.25 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Moseley, Jonathan D.; Gilday, John P.
Tetrahedron, 2006 , vol. 62, # 19 p. 4690 - 4697
参考文献
Gunnlaugsson, Thorfinnur; Kruger, Paul E.; Lee, T. Clive; Parkesh, Raman; Pfeffer, Frederick M.; Hussey, Gillian M.
Tetrahedron Letters, 2003 , vol. 44, # 35 p. 6575 - 6578
反应条件
sodium dichromate; acetic acid
Heating;
参考文献
Petrenko,G.P.; Ivanova,V.P.
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, # 5 p. 1065 - 1067,1074 - 1076
参考文献
Karischin; Kustol
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 692,693;engl.Ausg.S.673
反应条件
sulfolane; potassium carbonate in isopropyl alcohol
T=50 - 90°C; 3 h;
参考文献
3M INNOVATIVE PROPERTIES COMPANY
Patent: WO2004/24830 A1, 2004 ;
Location in patent: Page 25 ;
反应条件
sodium sulfide; sulfur in ethanol
3 h; Heating;
参考文献
Hekmatshoar; Beheshtiha; Nazari; Faridbod
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 7 p. 1521 - 1526
反应条件
in 2-ethoxy-ethanol
Substitution; 6 h; Heating;
参考文献
Minakova; Bedrik; Shershukov; Surov; Pivnenko
Chemistry of Heterocyclic Compounds, 1999 , vol. 35, # 5 p. 621 - 624
