1,3-二乙基-2-咪唑烷酮合成路线 （共 7 条）
反应条件
ClAu(di(tert-butyl)(1,1′-biphenyl-2-yl)-phosphine); silver trifluoromethanesulfonate in 1,4-dioxane
T=100°C; P=6205.94 Torr; 20 h; Autoclave;
参考文献
Zhang, Zhibin; Lee, Seong Du; Widenhoefer, Ross A.
Journal of the American Chemical Society, 2009 , vol. 131, p. 5372 - 5373
反应条件
1: With selenium
T=20°C; P=750.075 Torr; 2 h; neat (no solvent);
2: With oxygen
T=20°C; P=750.075 Torr; 1 h; neat (no solvent);
参考文献
Mizuno, Takumi; Nakai, Takeo; Mihara, Masatoshi
Synthesis, 2010 , # 24 art. no. F15510SS, p. 4251 - 4255
反应条件
1: imidazolidin-2-one With sodium hydride in N,N-dimethyl-formamide
T=20°C; 1.5 h;
2: ethyl iodide in N,N-dimethyl-formamide
T=20°C; 5 h;
参考文献
Suda, Koji; Saito, Noriko; Kumamoto, Takuya; Nakanishi, Waka; Kawahata, Masatoshi; Yamaguchi, Kentaro; Ogura, Yasumitsu; Suzuki, Kazuo T.; Ishikawa, Tsutomu
Heterocycles, 2009 , vol. 77, # 1 p. 375 - 387
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
5 h; Heating;
参考文献
Bogat-skii, A. V.; Luk'yanenko, N. G.; Kirichenko, T. I.; Limich, V. V.; Karpenko, L. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 89 - 95
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 1 p. 101 - 108
反应条件
potassium carbonate in benzene
1.) ice bath, 2 h; 2.) room temp., overnight;
参考文献
Cerioni, Giovanni; Cristiani, Franco; Devillanova, Francesco A.; Diaz, Angelo; Verani, Gaetano
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1983 , vol. 39, # 10 p. 929 - 932
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
5 h; Heating;
参考文献
Bogatsky, A. V.; Lukyanenko, N. G.; Kirichenko, T. I.
Synthesis, 1982 , # 6 p. 464 - 465
参考文献
Boon
Journal of the Chemical Society, 1947 , p. 313
Journal of the Chemical Society, 1956 , p. 5041
