N,N-二甲基苯胺-D6合成路线 （共 12 条）
反应条件
toluene-4-sulfonic acid in toluene 12 h; Reflux;
参考文献
Yang, Weicheng; Luo, Yong; Liu, Weixia; Deng, Xiaojun; Du, Xiaoning; Li, Meihua
Journal of Labelled Compounds and Radiopharmaceuticals, 2011 , vol. 54, # 4 p. 211 - 213
反应条件
sodium borodeuteride; sulfuric acid in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Dinnocenzo; Karki; Jones
Journal of the American Chemical Society, 1993 , vol. 115, # 16 p. 7111 - 7116
反应条件
1: aniline With tetra-(n-butyl)ammonium iodide; potassium hydroxide in water; benzene
T=20°C; 0.166667 h;
2: trideuteriomethyl iodide in water; benzene
T=20°C; 24.37 h; Reflux;
参考文献
Ratnikov, Maxim O.; Doyle, Michael P.
Journal of the American Chemical Society, 2013 , vol. 135, # 4 p. 1549 - 1557
反应条件
iron tribromide; 1,2,3,4,5-pentamethylcyclopentadiene; 5-oxopyrrolidine-(R)-2-carboxylic acid in 1,2,4-trimethyl benzene
T=200°C; 36 h; Inert atmosphere;
参考文献
Zhao, Yingsheng; Foo, Siong Wan; Saito, Susumu
Angewandte Chemie - International Edition, 2011 , vol. 50, # 13 p. 3006 - 3009
反应条件
tetrabutylammomium bromide; sodium hydroxide in water
T=70°C; 4 h;
参考文献
Yang, Weicheng; Luo, Yong; Liu, Weixia; Deng, Xiaojun; Du, Xiaoning; Li, Meihua
Journal of Labelled Compounds and Radiopharmaceuticals, 2011 , vol. 54, # 4 p. 211 - 213
反应条件
lithium triethylborohydride
参考文献
Pryor; Hendrickson Jr.
Journal of the American Chemical Society, 1983 , vol. 105, # 24 p. 7114 - 7122
反应条件
1: Heating
2: lithium triethylborohydride
View Scheme
参考文献
Pryor; Hendrickson Jr.
Journal of the American Chemical Society, 1983 , vol. 105, # 24 p. 7114 - 7122
反应条件
phosphorus pentoxide
T=150°C; 15 h;
参考文献
Peters, Kevin S.; Kim, Ganghyeok
Journal of Physical Chemistry A, 2004 , vol. 108, # 14 p. 2598 - 2606
反应条件
in methanol; acetonitrile
T=25°C; Rate constant;
参考文献
Zhang, Xiaoming; Yeh, Syun-Ru; Hong, Seok; Freccero, Mauro; Albini, Angelo; Falvey, Daniel E.; Mariano, Patrick S.
Journal of the American Chemical Society, 1994 , vol. 116, # 10 p. 4211 - 4220
反应条件
lithium aluminium deuteride
Multistep reaction;
参考文献
Weersink, Robert A.; Wallace, Stephen C.; Gordon, Robert D.
Journal of Chemical Physics, 1995 , vol. 103, # 22 p. 9530 - 9540
