N1,n2-二丁基乙烷-1,2-二胺合成路线 （共 18 条）
反应条件
transamination, boiling the reactants under nitrogene in inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Cragg, R. H.; Lappert, M. F.; Tilley, B. T.
Journal of the Chemical Society, 1964 , p. 2108 - 2115
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Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
hydrogen; (Co, Cu, Ni, Re, B)-containing catalyst/alumina
T=180°C; P=36030.5 Torr; 3 h; Autoclave; Product distribution / selectivity;
参考文献
Fazio, Michael J.; Molitor, Erich J.
Patent: US2011/92741 A1, 2011 ;
Location in patent: Page/Page column 5-6 ;
反应条件
hydrogen
T=180°C; P=34375.6 Torr; Autoclave; Product distribution / selectivity;
参考文献
Fazio, Michael J.; Molitor, Erich J.
Patent: US2011/92741 A1, 2011 ;
Location in patent: Page/Page column 5-6 ;
反应条件
1: T=20 - 60°C; Substitution;
2: With sodium hydroxide
T=20 - 25°C; Dehydrobromination;
参考文献
Serdyuk; Davydova; Chezlov; D'yakonov
Russian Journal of Applied Chemistry, 1999 , vol. 72, # 10 p. 1844 - 1845
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Rice et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 242,1750
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Rice et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 242,1750
反应条件
ethanol; potassium carbonate
Kochen des Reaktionsprodukts mit konz. HCl.;
参考文献
King; McMillan
Journal of the American Chemical Society, 1946 , vol. 68, p. 1776
参考文献
Donia et al.
Journal of Organic Chemistry, 1949 , vol. 14, p. 952,956, 960
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Zienty
Journal of the American Chemical Society, 1946 , vol. 68, p. 1388
反应条件
methanol; Pd-BaSO4
Hydrogenation;
参考文献
Epstein
Journal of Organic Chemistry, 1959 , vol. 24, p. 68,69
反应条件
hydrogen; platinum(IV) oxide
参考文献
Shepherd,R.G.; Wilkinson,R.G.
Journal of Medicinal and Pharmaceutical Chemistry, 1962 , vol. 5, p. 823 - 835
