3,3′-二甲氧基苯偶酰合成路线 （共 20 条）
反应条件
iron nitrate (III) 0.00833333 h; microwave irradiation;
参考文献
Zhao; Wang
Journal of Chemical Research - Part S, 2001 , # 2 p. 70 - 71
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=120°C; 1 h; Inert atmosphere;
参考文献
Kim, Ko Hoon; Park, Bo Ram; Lim, Jin Woo; Kim, Jae Nyoung
Tetrahedron Letters, 2011 , vol. 52, # 27 p. 3463 - 3466
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=60°C; 4 h; optical yield given as percent eeenantioselective reaction;
参考文献
Alamsetti, Santosh Kumar; Mannam, Sreedevi; Mutupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 5 p. 1086 - 1090
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; oxygen; copper(II) bis(trifluoromethanesulfonate); (R)-(+)-1,1'-binaphthyl-2,2'-diamine in toluene T=60°C; 6 h; optical yield given as percent eeenantioselective reaction;
参考文献
Alamsetti, Santosh Kumar; Mannam, Sreedevi; Mutupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 5 p. 1086 - 1090
反应条件
potassium permanganate; sodium hydrogencarbonate; magnesium sulfate in water; acetone T=20°C; 24 h;
参考文献
Trosien, Simon; Waldvogel, Siegfried R.
Organic Letters, 2012 , vol. 14, # 12 p. 2976 - 2979
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; 2,2'-bis(salicylideneamino)-1,1'-binaphthyl; oxygen; anhydrous cobalt diacetate in chloroform T=20°C; 55 h; Resolution of racemate; enantioselective reaction;
参考文献
Alamsetti, Santosh Kumar; Muthupandi, Pandi; Sekar, Govindasamy
Chemistry - A European Journal, 2009 , vol. 15, # 22 p. 5424 - 5427
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; n-dipropylamine / N,N-dimethyl-formamide / 16 h / 81 °C / Inert atmosphere 2: potassium permanganate; sodium hydrogencarbonate; magnesium sulfate / water; acetone / 24 h / 20 °C View Scheme
参考文献
Trosien, Simon; Waldvogel, Siegfried R.
Organic Letters, 2012 , vol. 14, # 12 p. 2976 - 2979
反应条件
Grubb's 2nd generation catalyst; tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; toluene; acetonitrile T=20°C; 1 h; Inert atmosphere; Reagent/catalystConcentrationTime;
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
反应条件
isocyanatocyclohexane in toluene Heating; Yield given;
参考文献
Cameron, James F.; Willson, C. Grant; Frechet, Jean M. J.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2429 - 2442
参考文献
US2014/128392 A1, ;
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