反应条件
1: (methoxymethyl)-triphenylphosphonium chloride With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.25 h; 2: 3,3-dimethyl-cyclohexanone in tetrahydrofuran; hexane T=0 - 20°C; 2 h; Further stages;
参考文献
AbbVie Inc.; Wang, Le; Doherty, George; Wang, Xilu; Tao, Zhi-Fu; Bruncko, Milan; Kunzer, Aaron R.; Wendt, Michael D.; Song, Xiaohong; Frey, Robin; Hansen, Todd M.; Sullivan, Gerard M.; Judd, Andrew; Souers, Andrew
Patent: US2013/96121 A1, 2013 ;
Location in patent: Paragraph 1544 ;