1-(3-羟基金刚烷-1-基)乙酮合成路线 (共 13 条)
参考文献
Daichel Chemical Industries Ltd
Patent: EP1000924 A1, 2000 ;
反应条件
oxygen; anhydrous cobalt diacetate in acetic acid T=60°C; Acylation; 2 h; Further byproducts given;
参考文献
Kishi, Arata; Kato, Susumu; Sakaguchi, Satoshi; Ishii, Yasutaka
Chemical Communications, 1999 , # 15 p. 1421 - 1422
反应条件
oxygen; anhydrous cobalt diacetate in acetic acid T=60°C; Acylation; 4 h; Further byproducts given;
参考文献
Kishi, Arata; Kato, Susumu; Sakaguchi, Satoshi; Ishii, Yasutaka
Chemical Communications, 1999 , # 15 p. 1421 - 1422
参考文献
Daicel Chemical Industries, Ltd.
Patent: US6429314 B1, 2002 ;
反应条件
oxygen; anhydrous cobalt diacetate in acetic acid T=60°C; Acylation; 2 h; Product distribution; Further Variations:CatalystsSolventstime of reaction;
参考文献
Kishi, Arata; Kato, Susumu; Sakaguchi, Satoshi; Ishii, Yasutaka
Chemical Communications, 1999 , # 15 p. 1421 - 1422
反应条件
sulfuric acid; acetic acid in water T=82°C; Decarboxylation;
参考文献
Pozdnyakov; Makarova; Moiseev
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 9 p. 1228 - 1231
反应条件
trichloromonobromomethane; water; molybdenum hexacarbonate T=150°C; 6 h; Inert atmosphere; regioselective reaction;
参考文献
Khusnutdinov; Shchadneva; Mukhametshina; Dzhemilev
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 8 p. 1137 - 1142
反应条件
1: sodium hydroxide / toluene / 1 h / 20 °C 2: acetic acid; water; sulfuric acid / 6 h / Heating View Scheme
参考文献
Makarova; Moiseev; Zemtsova
Russian Journal of General Chemistry, 1999 , vol. 69, # 4 p. 675 - 676
参考文献
Pozdnyakov; Moiseev
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 5 p. 739 - 741
反应条件
Yield given. Multistep reaction;
参考文献
Manchand; Cerruti; Martin; Hill; Merrett; Keech; Belshe; Connell; Sim
Journal of Medicinal Chemistry, 1990 , vol. 33, # 7 p. 1992 - 1995