1-氮杂双环[2.2.2]辛烷 盐酸盐合成路线 (共 8 条)
反应条件
potassium chloride; water in ethylene glycol dimethyl ether T=1°C; Rate constantProduct distribution;
参考文献
King; Hillhouse; Skonieczny
Canadian Journal of Chemistry, 1984 , vol. 62, # 10 p. 1977 - 1995
反应条件
potassium chloride; water in ethylene glycol dimethyl ether T=1°C; Rate constantProduct distribution;
参考文献
King; Hillhouse; Skonieczny
Canadian Journal of Chemistry, 1984 , vol. 62, # 10 p. 1977 - 1995
反应条件
in acetonitrile T=10°C; temperature, deuterated compound, isotope effect, ΔH(excit.), ΔS(excit.), ΔG(excit.); KineticsThermodynamic data;
参考文献
Dworniczak, Miroslaw; Jarczewski, Arnold
Acta Chimica Hungarica, 1989 , vol. 126, # 5 p. 599 - 604
反应条件
in diethyl ether byproducts: H2, LiCl; quinuclidine hydrochloride added over 5 min to an in situ generated soln. of LiInH4 contg. LiBr in Et2O at -78°C, warmed to -30°C,stirred for 2 h, filtered, kept at this temp. for 72 h; evapd. (vac.), extd. (toluene), crystd. at -50°C overnight;
参考文献
Cole, Marcus L.; Jones, Cameron; Kloth, Marc
Inorganic Chemistry, 2005 , vol. 44, # 14 p. 4909 - 4911
反应条件
potassium carbonate in methanol
参考文献
Leonik, Fedra M.; Papke, Roger L.; Horenstein, Nicole A.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 6 p. 1520 - 1522
反应条件
water; sodium hydroxide
参考文献
Wyman, Ian W.; Macartney, Donal H.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 1 p. 253 - 260
反应条件
water in water T=0°C; 3 h;
参考文献
Huang, Yifang; Parker, Michael H.; Reitz, Allen B.
Patent: US2007/14751 A1, 2007 ;
Location in patent: Page/Page column 9 ;
US 20070014751 A1
反应条件
in water T=0°C; 3 h;
参考文献
Huang, Yifang; Parker, Michael H.; Reitz, Allen B.
Patent: US2007/4715 A1, 2007 ;
Location in patent: Page/Page column 8 ;
US 20070004715 A1