反应条件
1: triethylamine / isopropyl alcohol / 2 h / 20 °C / |Inert atmosphere 2: triethylamine; Pd(PPh3)2Cl2; lithium chloride / N,N-dimethyl-formamide / 3 h / 130 °C / |Inert atmosphere; |Microwave irradiation; |Sealed tube 3: hydrogen; palladium 10 on activated carbon / methanol / 3 h / 20 °C 4: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Kabro, Anzhelika; Lachance, Hugo; Marcoux-Archambault, Iris; Perrier, Valerie; Dore, Vicky; Gros, Christina; Masson, Veronique; Gregoire, Jean-Marc; Ausseil, Frederic; Cheishvili, David; Laulan, Nathalie Bibens; St-Pierre, Yves; Szyf, Moshe; Arimondo, Paola B.; Gagnon, Alexandre
MedChemComm, 2013 , vol. 4, # 12 p. 1562 - 1570