1-丙-2-基氧基丙-2-醇合成路线 (共 7 条)
反应条件
Et3N-BH3; lithium perchlorate in diethyl ether
T=20°C; 1 h;
参考文献
Heydari, Akbar; Mehrdad, Morteza; Maleki, Aziz; Ahmadi, Nafiseh
Synthesis, 2004 , # 10 p. 1563 - 1565
参考文献
Chitwood; Freure
Journal of the American Chemical Society, 1946 , vol. 68, p. 680
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Dewael
Bulletin des Societes Chimiques Belges, 1930 , vol. 39, p. 399
反应条件
Al2O3/MgO composite
T=120°C; Inert atmosphere;
参考文献
Zhang, Yongbo; Lu, Bin; Wang, Xiaoguang; Zhao, Jingxiang; Cai, Qinghai
Applied Catalysis A: General, 2011 , vol. 408, # 1-2 p. 125 - 129
反应条件
boric acid trimethyl ester; hydrogen fluoride in water
0.5 h;
参考文献
SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
Patent: WO2006/34997 A1, 2006 ;
Location in patent: Page/Page column 19 ;
反应条件
lithium aluminium tetrahydride; boron trichloride
1.) CH2Cl2, 2 min, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
反应条件
sodium hydroxide
Heating; Yield given. Yields of byproduct given;
参考文献
Lee, Dae-Sil; Perlin, Arthur S.
Carbohydrate Research, 1982 , vol. 106, p. 1 - 20
反应条件
in isopropyl alcohol
参考文献
Chlebicki,J.
Roczniki Chemii, 1974 , vol. 48, p. 1241 - 1253