2,3-二羟基苯甲酸乙酯合成路线 （共 10 条）
反应条件
sulfuric acid in ethanol; water
参考文献
Syntex (USA) LLC
Patent: US6172062 B2, 2001 ;
US 6172062 B1
反应条件
sulfuric acid 24 h; Reflux;
参考文献
Mitsubishi Tanabe Pharma Corporation
Patent: EP2116538 A1, 2009 ;
Location in patent: Page/Page column 49 ;
反应条件
hydrogenchloride in ethanol; water T=60°C; 0.5 h;
参考文献
Bhujbal, Namdeo N.; Bande, Omprakash P.; Dhavale, Dilip D.
Carbohydrate Research, 2009 , vol. 344, # 6 p. 734 - 738
反应条件
hydrogenchloride in ethanol; water T=60°C; 0.5 h;
参考文献
Bhujbal, Namdeo N.; Bande, Omprakash P.; Dhavale, Dilip D.
Carbohydrate Research, 2009 , vol. 344, # 6 p. 734 - 738
反应条件
1: With trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78 - 20°C; 2: With hydrogenchloride in dichloromethane Further stages.;
参考文献
Sher, Muhammad; Tam Dang; Ahmed, Zafar; Rashid, Muhammad A.; Fischer, Christine; Langer, Peter
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6284 - 6286
参考文献
Albrecht, Markus; Mirtschin, Sebastian; De Groot, Marita; Janser, Ingo; Runsink, Jan; Raabe, Gerhard; Kogej, Michael; Schalley, Christoph A.; Froehlich, Roland
Journal of the American Chemical Society, 2005 , vol. 127, # 29 p. 10371 - 10387
反应条件
1: ammonium carbonate; water / 130 - 140 °C / im geschlossenen Rohr 2: H2SO4 View Scheme
参考文献
Praxmarer
Monatshefte fuer Chemie, 1906 , vol. 27, p. 1200
反应条件
potassium fluoride in N,N-dimethyl-formamide T=110°C; 14.5 h;
参考文献
Mitsubishi Tanabe Pharma Corporation
Patent: EP2116538 A1, 2009 ;
Location in patent: Page/Page column 49 ;
反应条件
hydrogenchloride; sodium chloride; potassium carbonate in water
参考文献
Syntex (USA) LLC
Patent: US6172062 B2, 2001 ;
US 6172062 B1
反应条件
lithium hydroxide in ethanol; water T=25°C; 2 h;
参考文献
Bhujbal, Namdeo N.; Bande, Omprakash P.; Dhavale, Dilip D.
Carbohydrate Research, 2009 , vol. 344, # 6 p. 734 - 738
