N'-(2-氰基-4-硝基苯基)-N,N-二甲基亚胺甲酰胺合成路线 （共 9 条）
反应条件
T=70°C; 0.0333333 h; Microwave irradiation;
参考文献
Foucourt, Alicia; Dubouilh-Benard, Carole; Chosson, Elizabeth; Corbiere, Cecile; Buquet, Catherine; Iannelli, Mauro; Leblond, Bertrand; Marsais, Francis; Besson, Thierry
Tetrahedron, 2010 , vol. 66, # 25 p. 4495 - 4502
反应条件
trichlorophosphate T=0 - 70°C;
参考文献
Wang, Zheng; Wang, Cuiling; Sun, Yanni; Zhang, Ning; Liu, Zhulan; Liu, Jianli
Tetrahedron, 2014 , vol. 70, # 4 p. 906 - 913
反应条件
1.1: sulfuric acid / 1.33 h / 50 - 65 °C 2.1: hydroxylamine hydrochloride / water / 0.5 h / |Reflux 2.2: 0.5 h 3.1: trichlorophosphate / 0 - 70 °C View Scheme
参考文献
Wang, Zheng; Wang, Cuiling; Sun, Yanni; Zhang, Ning; Liu, Zhulan; Liu, Jianli
Tetrahedron, 2014 , vol. 70, # 4 p. 906 - 913
反应条件
1.1: hydroxylamine hydrochloride / water / 0.5 h / |Reflux 1.2: 0.5 h 2.1: trichlorophosphate / 0 - 70 °C View Scheme
参考文献
Wang, Zheng; Wang, Cuiling; Sun, Yanni; Zhang, Ning; Liu, Zhulan; Liu, Jianli
Tetrahedron, 2014 , vol. 70, # 4 p. 906 - 913
反应条件
1.1: sodium sulfate; hydrogenchloride; hydroxylamine hydrochloride / water / 1 h / |Reflux 2.1: sulfuric acid / 1.33 h / 50 - 65 °C 3.1: hydroxylamine hydrochloride / water / 0.5 h / |Reflux 3.2: 0.5 h 4.1: trichlorophosphate / 0 - 70 °C View Scheme
参考文献
Wang, Zheng; Wang, Cuiling; Sun, Yanni; Zhang, Ning; Liu, Zhulan; Liu, Jianli
Tetrahedron, 2014 , vol. 70, # 4 p. 906 - 913
反应条件
acetic acid 3 h; Reflux;
参考文献
Wang, Zheng; Wang, Cuiling; Sun, Yanni; Zhang, Ning; Liu, Zhulan; Liu, Jianli
Tetrahedron, 2014 , vol. 70, # 4 p. 906 - 913
反应条件
in acetic acid Reflux;
参考文献
Xu, Yun-Yun; Li, Si-Ning; Yu, Gao-Jian; Hu, Qing-Hua; Li, Huan-Qiu
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 19 p. 6084 - 6091
反应条件
1: acetic acid / 2 h / Reflux 2: iron; acetic acid / ethanol; water / 70 - 80 °C View Scheme
参考文献
Li, Dong-Dong; Fang, Fei; Li, Jing-Ran; Du, Qian-Ru; Sun, Jian; Gong, Hai-Bin; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 18 p. 5870 - 5875
反应条件
in acetic acid T=148°C; 1.5 h;
参考文献
Wyeth Holdings Corporation
Patent: EP1000039 B1, 2004 ;
Location in patent: Page 34 ;
