4-甲氧基-4'-甲基二苯胺合成路线 （共 37 条）
反应条件
[(CyPF-tBu)PdCl2]; sodium t-butanolate in ethylene glycol dimethyl ether T=110°C; 48 h; Inert atmosphereSealed vial;
参考文献
Shen, Qilong; Hartwig, John F.
Organic Letters, 2008 , vol. 10, # 18 p. 4109 - 4112
反应条件
potassium carbonate in water T=20°C;
参考文献
Sawant, Sanghapal D.; Srinivas, Mahesuni; Aravinda Kumar; Lakshma Reddy; Singh, Parvinder Pal; Singh, Baldev; Sharma, Amit Kumar; Sharma; Vishwakarma, Ram A.
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5351 - 5354
反应条件
potassium hydroxide; tert-butyl alcohol; cyclopalladated ferrocenylimine monophosphinobiaryl complex in water T=95°C; Buchwald-Hartwig amination; 24 h;
参考文献
Xu, Chen; Gong, Jun-Fang; Wu, Yang-Jie
Tetrahedron Letters, 2007 , vol. 48, # 9 p. 1619 - 1623
反应条件
tris(dibenzylideneacetone)dipalladium (0); sodium t-butanolate; Verkade nonionic superbase in toluene Heating;
参考文献
Shen, Huafeng; Zhang, Zhong-Ping; Li, Jing-Hua
Journal of Chemical Research, 2010 , # 3 p. 163 - 166
反应条件
cBRIDP; bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate in water T=20°C; 21 h; Inert atmosphereMicellar solution;
参考文献
Lipshutz, Bruce H.; Chung, David W.; Rich, Brian
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1717 - 1721
反应条件
triethylamine; cupric acetate immobilized onto Wang resin in dichloromethane T=20°C; 24 h;
参考文献
Zhu, Xingyi; Zhang, Qihong; Su, Weike
RSC Advances, 2014 , vol. 4, # 43 p. 22775 - 22778
反应条件
sodium t-butanolate in 1,4-dioxane T=100°C; 8 h;
参考文献
Takasago International Corporation
Patent: EP1167372 A1, 2002 ;
Location in patent: Example 27 ;
反应条件
tetrabutylammomium bromide; oxygen; palladium diacetate in dimethyl sulfoxide T=90°C; P=760.051 Torr; 12 h; Schlenk techniqueMolecular sieveInert atmosphere; SolventReagent/catalyst;
参考文献
Hajra, Alakananda; Wei, Ye; Yoshikai, Naohiko
Organic Letters, 2012 , vol. 14, # 21 p. 5488 - 5491,4
反应条件
biphenyl-2-yl-di-tert-butyl-phosphane; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium (0) in toluene T=20°C; Arylation; 48 h;
参考文献
Wolfe, John P.; Tomori, Hiroshi; Sadighi, Joseph P.; Yin, Jingjun; Buchwald, Stephen L.
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1158 - 1174
反应条件
in anhydrous xylene T=140°C; Inert atmosphere;
参考文献
Ou, Lili; Shao, Jiaan; Zhang, Guolin; Yu, Yongping
Tetrahedron Letters, 2011 , vol. 52, # 13 p. 1430 - 1431
