4’-氯-2-硝基二苯醚合成路线 (共 10 条)
反应条件
CsCO3 in dimethyl sulfoxide T=80°C; Substitution; 20 h;
参考文献
Dinsmore, Christopher J.; Zartman, C. Blair
Tetrahedron Letters, 1999 , vol. 40, # 21 p. 3989 - 3990
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in water; dimethyl sulfoxide T=80°C; 2 h;
参考文献
Yeom, Chang-Eun; Kim, Hye Won; Lee, So Young; Kim, B. Moon
Synlett, 2007 , # 1 p. 146 - 150
反应条件
potassium fluoride supported on Clinoptilolite in dimethyl sulfoxide T=110 - 115°C; 2 h;
参考文献
Khalilzadeh, Mohammad A.; Hosseini, Abolfazl; Pilevar, Afsaneh
European Journal of Organic Chemistry, 2011 , # 8 p. 1587 - 1592
参考文献
Golinske, Dirk; Voss, Juergen; Adiwidjaja, Gunadi
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 6 p. 862 - 880
反应条件
caesium carbonate in dimethyl sulfoxide 0.133333 h; microwave irradiation;
参考文献
Xu, Hui; Chen, Yang
Synthetic Communications, 2007 , vol. 37, # 14 p. 2411 - 2420
参考文献
Bayer Aktiengesellschaft
Patent: US5382686 A1, 1995 ;
反应条件
chlorine; acetic acid
参考文献
McCombie; Macmillan; Scarborough
Journal of the Chemical Society, 1931 , p. 529,533
参考文献
Henley
Journal of the Chemical Society, 1930 , p. 1222
Full Text Show Details
McCombie; Macmillan; Scarborough
Journal of the Chemical Society, 1931 , p. 529,533
反应条件
1: With iron; ammonium chloride in ethanol; water 1 h; Heating / reflux; 2: With water; sodium hydrogencarbonate Product distribution / selectivity;
参考文献
STERIX LIMITED
Patent: WO2007/3934 A2, 2007 ;
Location in patent: Page/Page column 119 ;
WO 2007/003934 A2
反应条件
2: NaNO2; HCl; sulfuric acid
View Scheme
参考文献
McCombie; Macmillan; Scarborough
Journal of the Chemical Society, 1931 , p. 529,533