1-(4-甲氧基苯基)-2-(4-硝基苯基)-乙炔合成路线 (共 24 条)
反应条件
1: 94 percent / dimethylformamide / 16 h / 20 °C
2: 92 percent / Br2 / CH2Cl2 / 16 h
3: 95 percent / KOtBu / 2-methyl-propan-2-ol / 5 h / 50 °C
View Scheme
参考文献
Pati, Hari N.; Wicks, Martha; Holt Jr., Herman L.; LeBlanc, Regan; Weisbruch, Paul; Forrest, Lori; Lee, Moses
Heterocyclic Communications, 2005 , vol. 11, # 2 p. 117 - 120
反应条件
1: 65 percent / tetrahydrofuran / 3 h / Ambient temperature
2: 84 percent / POCl3, N,N-diethylaniline / 1 h / 90 °C
3: 58 percent / t-BuOK / tetrahydrofuran / 3 h / Ambient temperature
View Scheme
参考文献
Kondo, Koichi; Fujitani, Takumi; Ohnishi, Noriaki
Journal of Materials Chemistry, 1997 , vol. 7, # 3 p. 429 - 433
反应条件
1: 84 percent / POCl3, N,N-diethylaniline / 1 h / 90 °C
2: 58 percent / t-BuOK / tetrahydrofuran / 3 h / Ambient temperature
View Scheme
参考文献
Kondo, Koichi; Fujitani, Takumi; Ohnishi, Noriaki
Journal of Materials Chemistry, 1997 , vol. 7, # 3 p. 429 - 433
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
1.5 h; Ambient temperature;
参考文献
Akiyama, Shuzo; Nakatsuji, Shin'ichi; Nomura, Kimiko; Matsuda, Kosei; Nakashima, Kenichiro
Journal of the Chemical Society, Chemical Communications, 1991 , # 14 p. 948 - 950