2,4,5-三甲氧基苯丙酮合成路线 （共 13 条）
反应条件
1: MeONO, HCl 2: aq. H2SO4 View Scheme
参考文献
Hardegger,E. et al.
Helvetica Chimica Acta, 1964 , vol. 47, p. 1996 - 2017
反应条件
1: 100 percent / NaBH4 / ethanol / 1 h / 20 °C 2: 95 percent / AcONa; Ac2O / 3 h / Heating View Scheme
参考文献
Diaz, Francisco; Contreras, Leticia; Flores, Rosa; Tamariz, Joaquin; Labarrios, Fernando; et al.
Organic Preparations and Procedures International, 1991 , vol. 23, # 2 p. 133 - 138
反应条件
formic acid; water; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane
T=110 - 120°C; 0.266667 h; microwave irradiation;
参考文献
Joshi, Bhupendra P.; Sharma, Anuj; Sinha, Arun K.
Canadian Journal of Chemistry, 2005 , vol. 83, # 10 p. 1826 - 1832
反应条件
aluminium trichloride in dichloromethane
T=10°C; 1 h;
参考文献
Hoegberg, Thomas; Bengtsson, Stefan; Paulis, Tomas de; Johansson, Lars; Stroem, Peter; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 4 p. 1155 - 1163
反应条件
bunazosin in 1,4-dioxane; ethanol
参考文献
Council of Scientific and Industrial Research
Patent: US6590127 B1, 2003 ;
反应条件
iodine
T=70°C; Acylation; 6 h;
参考文献
Diaz, Francisco; Contreras, Leticia; Flores, Rosa; Tamariz, Joaquin; Labarrios, Fernando; et al.
Organic Preparations and Procedures International, 1991 , vol. 23, # 2 p. 133 - 138
参考文献
Council of Scientific and Industrial Research
Patent: US6590127 B1, 2003 ;
反应条件
PPA
T=45 - 50°C; 4 h;
参考文献
Sanchez-Viesca; Gomez; Berros, Martha
Heterocyclic Communications, 2003 , vol. 9, # 4 p. 367 - 372
反应条件
1: methanol; NaOH-solution
2: CS2; AlCl3
View Scheme
参考文献
Bargellini; Martegiani
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1911 , vol. <5> 20 II, p. 18,21
Gazzetta Chimica Italiana, 1911 , vol. 41 II, p. 445,449
参考文献
Paolini
Gazzetta Chimica Italiana, 1910 , vol. 40 I, p. 114
