4-甲基-N-(丙-2-亚基氨基)苯磺酰胺合成路线 （共 11 条）
反应条件
(i) nBuLi, (ii) MeLi; Multistep reaction;
参考文献
Lipton,M.F.; Shapiro,R.H.
Journal of Organic Chemistry, 1978 , vol. 43, # 7 p. 1409 - 1413
反应条件
acetic acid; zinc T=25°C; Inert atmosphere;
参考文献
Emmett, Edward J.; Richards-Taylor, Charlotte S.; Nguyen, Bao; Garcia-Rubia, Alfonso; Hayter, Barry R.; Willis, Michael C.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 20 p. 4007 - 4014
反应条件
in methanol
T=20°C; Inert atmosphere;
参考文献
Allwood, Daniel M.; Blakemore, David C.; Ley, Steven V.
Organic Letters, 2014 , vol. 16, # 11 p. 3064 - 3067
反应条件
Pearlman's catalist; hydrogen in acetone
T=25°C; 16 h;
参考文献
Emmett, Edward J.; Richards-Taylor, Charlotte S.; Nguyen, Bao; Garcia-Rubia, Alfonso; Hayter, Barry R.; Willis, Michael C.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 20 p. 4007 - 4014
反应条件
sodium hydride in diethylene glycol dimethyl ether
参考文献
Ulman,A.; Sprecher,M.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3703 - 3707
反应条件
1: acetic acid
2: NaH / bis-(2-methoxy-ethyl) ether
View Scheme
参考文献
Ulman,A.; Sprecher,M.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3703 - 3707
反应条件
1: 1,4-diaza-bicyclo[2.2.2]octane; (DABCO)*(SO2)2; palladium diacetate; [(t-Bu)3PH]BF4 / 1,4-dioxane / 16 h / 70 °C / Inert atmosphere
2: Pearlman's catalist; hydrogen / acetone / 16 h / 25 °C
View Scheme
参考文献
Emmett, Edward J.; Richards-Taylor, Charlotte S.; Nguyen, Bao; Garcia-Rubia, Alfonso; Hayter, Barry R.; Willis, Michael C.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 20 p. 4007 - 4014
参考文献
Borsche; Frank
Justus Liebigs Annalen der Chemie, 1926 , vol. 450, p. 79
参考文献
McDonald,R.M.; Krueger,R.A.
Journal of Organic Chemistry, 1966 , vol. 31, p. 488 - 494
反应条件
potassium superoxide in acetonitrile
T=-30°C; 7 h;
参考文献
Kim, Yong Hae; Lee, Hyeon Kyu; Chang, Hae Sung
Tetrahedron Letters, 1987 , vol. 28, # 37 p. 4285 - 4288
