6-甲氧基-2-乙酰萘合成路线 (共 124 条)
反应条件
water; silver trifluoromethanesulfonate 5.5 h; Heating;
参考文献
Das, Rima; Chakraborty, Debashis
Applied Organometallic Chemistry, 2012 , vol. 26, # 12 p. 722 - 726
反应条件
hydrogenchloride; sodium hydroxide; aluminium trichloride in water; toluene
参考文献
Alfa Chemicals Italiana S.r.l.
Patent: EP440930 A2, 1991 ;
反应条件
aluminium trichloride in dichloromethane T=25°C; 12 h;
参考文献
Nandanan; Jayachandran; Phukan, Prodeep; Pais, Godwin C. G.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 12 p. 1221 - 1227
反应条件
Magtrievetrade; in acetonitrile T=135°C; Fixed-bed flow reactorInductive heatingHigh pressure;
参考文献
Henkel AG and Co. KGaA
Patent: US2011/301363 A1, 2011 ;
Location in patent: Page/Page column 6-7 ;
反应条件
triethylamine; palladium in tetrahydrofuran T=65°C; P=15200 Torr; 17 h;
参考文献
Hiyama; Wakasa; Ueda; Kusumoto
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 2 p. 640 - 642
参考文献
Nobel Chemicals AB
Patent: EP176142 B1, 1991 ;
反应条件
oxygen; (-)-sparteine; palladium diacetate in toluene T=80°C; P=760 Torr;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
aluminium trichloride
参考文献
Alfa Wassermann S.p.A.
Patent: US5107013 A1, 1992 ;
反应条件
1: With oxygen; (-)-sparteine; palladium diacetate in toluene T=80°C; P=760 Torr; 2: With pyridine; phosphorus tribromide in diethyl ether T=-20 - 0°C; Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562
反应条件
1: R-1-[6-methoxy-2-naphthyl]-hydroxyethane With oxygen; (-)-sparteine; palladium diacetate in toluene T=80°C; P=760 Torr; 2: With pyridine; phosphorus tribromide in diethyl ether T=-20 - 0°C; 3: sodium cyanide in N,N-dimethyl-formamide T=80°C; Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 3 p. 557 - 562