1-O-辛基-β-D-吡喃葡萄糖苷2,3,4,6-四乙酸盐合成路线 （共 26 条）
反应条件
metal carbonates in neat (no solvent) 3 h; Milling;
参考文献
Tyagi, Mohit; Khurana, Darpan; Ravindranathan Kartha
Carbohydrate Research, 2013 , vol. 379, p. 55 - 59
反应条件
iodine in acetonitrile T=25°C; chemoselective reaction;
参考文献
Dutta, Samrat; Sarkar, Swarbhanu; Gupta, Shyam Ji; Sen, Asish Kumar
Tetrahedron Letters, 2013 , vol. 54, # 8 p. 865 - 870
反应条件
sodium tetrahydroborate in dimethyl sulfoxide T=20°C; 1 h;
参考文献
Akita, Hiroyuki; Kawahara, Eiji; Kato, Keisuke
Tetrahedron Asymmetry, 2004 , vol. 15, # 10 p. 1623 - 1629
反应条件
1: octyl 2,3,4-tri-O-acetyl-6-O-trityl-β-D-glucopyranoside With hydrogen; palladium on activated charcoal in methanol T=20°C; 2: 2,3,4-tri-O-acetyl-α-D-arabinopyranosyl bromide With silver trifluoromethanesulfonate; N,N,N',N'-tetramethyl-urea in dichloromethane T=20°C; 0.5 h;
参考文献
Akita, Hiroyuki; Kawahara, Eiji; Kato, Keisuke
Tetrahedron Asymmetry, 2004 , vol. 15, # 10 p. 1623 - 1629
反应条件
1: glucose pentaacetate; octanol With zinc(II) chloride T=115°C; 0.05 h; microwave irradiation; 2: acetic anhydride With pyridine T=20°C; Further stages.;
参考文献
Ferlin, Nadege; Grassi, Diego; Ojeda, Carlos; Castro, Mariano J.L.; Grand, Eric; Fernandez Cirelli, Alicia; Kovensky, Jose
Carbohydrate Research, 2008 , vol. 343, # 5 p. 839 - 847
反应条件
4 A molecular sieve; tin(IV) chloride in dichloromethane T=20°C; 4 h;
参考文献
Droz, Anne Sophie; Neidlein, Ulf; Anderson, Sally; Seiler, Paul; Diederich, Francois
Helvetica Chimica Acta, 2001 , vol. 84, # 8 p. 2243 - 2289
反应条件
4 A molecular sieve; tin(IV) chloride in dichloromethane T=20°C; 1 h;
参考文献
Konstantinovic; Predojevic; Mojsilovic; Dimitrijevic; Milosevic
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 9 p. 796 - 801
反应条件
Fe-β zeolite T=140°C; Helferich glycosylation; 14 h;
参考文献
Aich, Udayanath; Loganathan, Duraikkannu
Carbohydrate Research, 2007 , vol. 342, # 5 p. 704 - 709
反应条件
boron trifluoride diethyl etherate in dichloromethane T=20°C; 100 h;
参考文献
Petrovic, Zorica; Konstantinovic, Stanimir; Spasojevic, Aleksandra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 1 p. 132 - 134
反应条件
1: D-glucopyranose; octanol With iron(III) chloride; calcium chloride in 1,4-dioxane T=20°C; 24 h; 2: acetic anhydride With pyridine T=100°C; 1 h;
参考文献
Jerkovic, Igor; Mastelic, Josip; Blazevic, Ivica; Sindler-Kulyk, Marija; Vikic-Topic, Drazen
Croatica Chemica Acta, 2005 , vol. 78, # 2 p. 313 - 318
