苯甲酸-Alpha-13C合成路线 （共 27 条）
反应条件
thionyl chloride; tetrahydrogenoboratebis(triphenylphosphine)copper(I); triphenylphosphine 1.) benzene, reflux, 3 h, 2.) tetraglyme, RT, 3.5 h; Yield given. Multistep reaction;
参考文献
Yamataka, Hiroshi; Sasaki, Daizo; Kuwatani, Yoshiyuki; Mishima, Masaaki; Tsuno, Yuho
Journal of the American Chemical Society, 1997 , vol. 119, # 42 p. 9975 - 9979
反应条件
1: SOCl2 2: Na2O2 View Scheme
参考文献
Takeuchi, Ken'ichi; Murai, Osamu; Matsui, Shin; Inoue, Takeshi; Kitagawa, Toshikazu; Okamoto, Kunio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1301 - 1310
反应条件
1: SOCl2 2: Na2O2 3: 1,2-dichloro-ethane / 840 h / 50 °C View Scheme
参考文献
Takeuchi, Ken'ichi; Murai, Osamu; Matsui, Shin; Inoue, Takeshi; Kitagawa, Toshikazu; Okamoto, Kunio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1301 - 1310
反应条件
in diethyl ether T=20°C; 2 h;
参考文献
Haiss, Peter; Zeller, Klaus-Peter
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2003 , vol. 58, # 6 p. 595 - 605
反应条件
1: [carbonyl-13C] benzoic acid in thionyl chloride 2 h; Reflux; 2: benzene With AlCl3, aluminium chloride T=40°C; 14 h; Inert atmosphere;
参考文献
Siu, Paul W.; Serin, Spencer C.; Krummenacher, Ivo; Hey, Thomas W.; Gates, Derek P.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6967 - 6970
Angew. Chem., 2013 , vol. 125, # 27 p. 7105 - 7108,4
反应条件
1: SOCl2 2: AlCl3 View Scheme
参考文献
Knaap, Th.A. van der; Klebach, Th.C.; Visser, F.; Bickelhaupt, F.; Ros, P.; et al.
Tetrahedron, 1984 , vol. 40, # 4 p. 765 - 776
参考文献
Casey, Charles P.; Scheck, Daniel M.
Journal of the American Chemical Society, 1980 , vol. 102, # 8 p. 2728 - 2731
参考文献
Apeloig, Yitzhak; Franke, Wilfried; Rappoport, Zvi; Schwarz, Helmut; Stahl, Daniel
Journal of the American Chemical Society, 1981 , vol. 103, # 10 p. 2770 - 2780
参考文献
Brown, John M.; Chaloner, Penny A.
Journal of the American Chemical Society, 1980 , vol. 102, # 9 p. 3040 - 3048
反应条件
sulfated zirconia
P=452 Torr; 120 h; Ambient temperature;
参考文献
Clingenpeel, T. H.; Wessel, T. E.; Biaglow, A. I.
Journal of the American Chemical Society, 1997 , vol. 119, # 23 p. 5469 - 5470
