3-(3-乙氧基-2-甲基-3-氧代丙基)偶氮-2-甲基丙酸乙酯合成路线 （共 8 条）
参考文献
Thiele; Heuser
Justus Liebigs Annalen der Chemie, 1896 , vol. 290, p. 22
反应条件
1: With chlorine; sodium bromide in toluene
T=20°C; 2 h;
2: With hydrogenchloride in toluene
T=20°C; 3 h;
3: With water in toluene
T=25 - 30°C; 1 h;
参考文献
Atofina
Patent: US6407219 B1, 2002 ;
Location in patent: Page column 9 ;
反应条件
1: With hydrogenchloride in toluene
T=15 - 20°C; 20 - 21 h;
2: With water in toluene
T=30°C; 2 h;
参考文献
Atofina
Patent: US6407219 B1, 2002 ;
Location in patent: Page column 9 - 10 ;
反应条件
water
T=10 - 30°C; 1 h;
参考文献
Atofina
Patent: US6407219 B1, 2002 ;
Location in patent: Page column 7 - 8 ;
反应条件
1:
2: With hydrogenchloride
参考文献
Atofina
Patent: US6407219 B1, 2002 ;
Location in patent: Page column 9 ;
参考文献
Rohm and Haas Co.
Patent: US2713576 , 1949 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Rohm and Haas Co.
Patent: DE849109 , 1951 ;
参考文献
Bizilj, Snezna; Kelly, David P.; Serelis, Algirdas K.; Solomon, David H.; White, Kathleen E.
Australian Journal of Chemistry, 1985 , vol. 38, # 11 p. 1657 - 1673
反应条件
1: HCl / 18 h / 5 °C
2: water / 0.5 h
View Scheme
参考文献
Bizilj, Snezna; Kelly, David P.; Serelis, Algirdas K.; Solomon, David H.; White, Kathleen E.
Australian Journal of Chemistry, 1985 , vol. 38, # 11 p. 1657 - 1673
