反应条件
1: bis(η3-allyl-μ-chloropalladium(II)); 1,2-bis-(diphenylphosphino)ethane; N,O-bis-(trimethylsilyl)-acetamide; sodium acetate / tetrahydrofuran / 40 h / 70 °C / |Inert atmosphere
2: water; acetic acid / 4 h / 100 °C
3: R-(+)-prolinamide; pyridinium p-toluenesulfonate / acetonitrile / 12 h / 80 °C / |Inert atmosphere
View Scheme
参考文献
Trzoss, Lynnie; Xu, Jing; Lacoske, Michelle H.; Mobley, William C.; Theodorakis, Emmanuel A.
Chemistry - A European Journal, 2013 , vol. 19, # 20 p. 6398 - 6408