3-(二甲氨基)丙酸甲酯合成路线 （共 26 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
TAKASAGO INTERNATIONAL CORPORATION
Patent: US2010/63294 A1, 2010 ;
Location in patent: Page/Page column 14 ;
反应条件
hydrogen fluoride T=7 - 8°C; 9.11667 h; electrolysis (3.5 A/dm2, 6.0 to 6.1 V); Further byproducts given;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Fukaya, Haruhiko
Journal of Fluorine Chemistry, 1990 , vol. 48, # 2 p. 257 - 279
反应条件
hydrogen fluoride T=7 - 8°C; 9.11667 h; electrolysis (3.5 A/dm2, 6.0 to 6.1 V); Further byproducts given;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Fukaya, Haruhiko
Journal of Fluorine Chemistry, 1990 , vol. 48, # 2 p. 257 - 279
反应条件
hydrogen fluoride T=7 - 8°C; 9.11667 h; electrolysis (3.5 A/dm2, 6.0 to 6.1 V); Further byproducts given;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Fukaya, Haruhiko
Journal of Fluorine Chemistry, 1990 , vol. 48, # 2 p. 257 - 279
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 95, p. 341
反应条件
diethyl ether und Behandeln des Reaktionsgemisches mit wss.Ammoniumchlorid-Loesung;
参考文献
Nasarow; Kruglikowa
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 346,353; engl. Ausg. S. 387, 394
反应条件
multistep reaction, other alkyl and cycloalkyl halogenides, use as synthetic equivalent of acrylic acid α anion;
参考文献
Yu, Lin-Chen; Helquist, Paul
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4536 - 4541
反应条件
1: methyl 3-(dimethylamino)-propanoate With lithium diisopropyl amide in tetrahydrofuran; n-heptane; ethylbenzene T=-30°C; Inert atmosphere; 2: 4-bromo-benzyl bromide in tetrahydrofuran; n-heptane; ethylbenzene T=-30 - -15°C; Inert atmosphere;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 52, # 1 p. 23 - 28
反应条件
(i) LDA, (ii) /BRN= 969135/, HMPT; Multistep reaction;
参考文献
Tetrahedron Letters, , p. 3423 - 3426
参考文献
Chemische Berichte, , vol. 35, p. 602
