1,3,5-三-氯甲基-2,4,6-三甲基-苯合成路线 （共 10 条）
反应条件
(i) (pyrolysis), (ii) Br2, CHCl3; Multistep reaction;
参考文献
Schiess,P.; Heitzmann,M.
Helvetica Chimica Acta, 1978 , vol. 61, p. 844 - 847
反应条件
in acetone 15 h; Heating; Yield given;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
tin(IV) chloride
T=20°C;
参考文献
Roelens, Stefano; Vacca, Alberto; Francesconi, Oscar; Venturi, Chiara
Chemistry - A European Journal, 2009 , vol. 15, # 33 p. 8296 - 8302
反应条件
hydrogenchloride; sodium chloride; zinc(II) chloride
29 h; Heating;
参考文献
Choi, Heung-Jin; Park, Yeon Sil; Yun, Seok Hun; Kim, Hong-Seok; Cho, Chan Sik; Ko, Kwangnak; Ahn, Kyo Han
Organic letters, 2002 , vol. 4, # 5 p. 795 - 798
反应条件
hydrogenchloride; epoxysulfonyl fluoride; lead dioxide
1. -75 grad C 2. - 40 grad C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
hydrogenchloride; epoxysulfonyl fluoride; lead dioxide
1. 75 grad C, 2- 3,5 h 2. - 60 grad C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
hydrogenchloride
2 h; Heating; Title compound not separated from byproducts.;
参考文献
Zenkevich; Makarov
Russian Journal of General Chemistry, 2007 , vol. 77, # 4 p. 611 - 619
反应条件
epoxysulfonyl fluoride; lead dioxide
T=-75 - -70°C; 2 h; different conc. PbO2, different time, decomposition reagent CH3OH or HCl conc.; MechanismProduct distribution;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
epoxysulfonyl fluoride; lead dioxide
T=-75 - -70°C; 2 h; different conc. PbO2, different time, decomposition reagent CH3OH or HCl conc.; MechanismProduct distribution;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
参考文献
Schiess,P.; Heitzmann,M.
Helvetica Chimica Acta, 1978 , vol. 61, p. 844 - 847
