ALPHA-氯-4-甲氧基苯甲醛肟合成路线 (共 51 条)
反应条件
triethylamine in ethanol
T=20°C;
参考文献
Zamponi, Gerald W.; Stotz, Stephanie C.; Staples, Richard J.; Andro, Tina M.; Nelson, Jared K.; Hulubei, Victoria; Blumenfeld, Alex; Natale, Nicholas R.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 1 p. 87 - 96
反应条件
triethylamine in diethyl ether
48 h; Ambient temperature;
参考文献
Albini, Franca Marinone; Franco, Rita De; Bandiera, Tiziano; Caramella, Pierluigi; Corsaro, Antonino; Perrini, Giancarlo
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 757 - 761
参考文献
Kinney et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 3418,3421
参考文献
Kinney et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 3418,3421
参考文献
Kinney et al.
Journal of the American Chemical Society, 1933 , vol. 55, p. 3418,3421
反应条件
(i) Et3N, (ii) /BRN= 1851372/, benzene; Multistep reaction;
参考文献
Bianchi,G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1518 - 1523
反应条件
(i) Et3N, (ii) /BRN= 1851372/, benzene; Multistep reaction;
参考文献
Bianchi,G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1518 - 1523
反应条件
1: With triethylamine in trichloroethane, 1,1,2-
0.5 h; Heating;
2: With sodium hydroxide
0.5 h; Heating;
参考文献
Schofield, Mark H.; Sorel, Marie-Adele; Manalansan, Ryan J.; Richardson, David P.; Markgraf, J. Hodge
Magnetic Resonance in Chemistry, 2006 , vol. 44, # 9 p. 851 - 855
反应条件
1: 86 percent / triethylamine / CH2Cl2 / 6 h / 20 °C
2: CH3I; NaI / dimethylformamide / 20 h / 80 °C
3: DBU / tetrahydrofuran; dimethylformamide / 10 h / 90 °C
View Scheme
参考文献
Xu, Wei Ming; Tang; Huang, Xian
Tetrahedron, 2005 , vol. 61, # 2 p. 501 - 506
参考文献
Salgado-Zamora, Hector; Campos, Elena; Jimenez, Rogelio; Cervantes, Humberto
Heterocycles, 1998 , vol. 47, # 2 p. 1043 - 1049